X-ray photoelectron spectroscopy study of Pd oxidation by RF discharge in oxygen
Publication type: Journal Article
Publication date: 2009-08-01
scimago Q1
wos Q1
SJR: 1.310
CiteScore: 13.4
Impact factor: 6.9
ISSN: 01694332, 18735584
Surfaces, Coatings and Films
General Chemistry
General Physics and Astronomy
Condensed Matter Physics
Surfaces and Interfaces
Abstract
The low-temperature oxidation of polycrystalline palladium by RF oxygen plasma was studied via X-ray photoelectron spectroscopy (XPS) and scanning electron microscopy (SEM). Detailed information about the electronic states of palladium and oxygen was obtained based on the XPS curve fitting analysis of Pd3d and Pd3p + O1s lines. The results showed that Pd oxidation by oxygen plasma was different from Pd oxidation in pure O2 at high temperature. SEM shows well-structured submicron PdO particles result from oxidation in pure O2, whereas plasma oxidation results in the predominant formation of two-dimensional PdO structures covering the initial crystallites of the Pd foil. Further oxidation to a three-dimensional PdO phase occurs under prolonged treatment with oxygen plasma. The formation of a PdOx (x > 1) species, characterized by a Eb(Pd3d5/2) = 338.0–338.2 eV value that is close to the Pd4+ oxidation state, was also observed. This PdOx species was found to have low thermal stability (T
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177
Total citations:
177
Citations from 2024:
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(16%)
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Kibis L. et al. X-ray photoelectron spectroscopy study of Pd oxidation by RF discharge in oxygen // Applied Surface Science. 2009. Vol. 255. No. 22. pp. 9248-9254.
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Kibis L., Titkov A. I., Stadnichenko A., Koscheev S., Boronin A. X-ray photoelectron spectroscopy study of Pd oxidation by RF discharge in oxygen // Applied Surface Science. 2009. Vol. 255. No. 22. pp. 9248-9254.
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TY - JOUR
DO - 10.1016/j.apsusc.2009.07.011
UR - https://doi.org/10.1016/j.apsusc.2009.07.011
TI - X-ray photoelectron spectroscopy study of Pd oxidation by RF discharge in oxygen
T2 - Applied Surface Science
AU - Kibis, Lidiya
AU - Titkov, A I
AU - Stadnichenko, Andrey
AU - Koscheev, S.V.
AU - Boronin, Andrei
PY - 2009
DA - 2009/08/01
PB - Elsevier
SP - 9248-9254
IS - 22
VL - 255
SN - 0169-4332
SN - 1873-5584
ER -
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BibTex (up to 50 authors)
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@article{2009_Kibis,
author = {Lidiya Kibis and A I Titkov and Andrey Stadnichenko and S.V. Koscheev and Andrei Boronin},
title = {X-ray photoelectron spectroscopy study of Pd oxidation by RF discharge in oxygen},
journal = {Applied Surface Science},
year = {2009},
volume = {255},
publisher = {Elsevier},
month = {aug},
url = {https://doi.org/10.1016/j.apsusc.2009.07.011},
number = {22},
pages = {9248--9254},
doi = {10.1016/j.apsusc.2009.07.011}
}
Cite this
MLA
Copy
Kibis, Lidiya, et al. “X-ray photoelectron spectroscopy study of Pd oxidation by RF discharge in oxygen.” Applied Surface Science, vol. 255, no. 22, Aug. 2009, pp. 9248-9254. https://doi.org/10.1016/j.apsusc.2009.07.011.