volume 74 pages 128940

Synthesis and biological testing of 3,5-bis(arylidene)-4-piperidone conjugates with 2,5-dihydro-5H-1,2-oxaphospholenes

Publication typeJournal Article
Publication date2022-10-01
scimago Q2
wos Q2
SJR0.472
CiteScore5.1
Impact factor2.2
ISSN0960894X, 14643405
Organic Chemistry
Drug Discovery
Biochemistry
Molecular Biology
Pharmaceutical Science
Clinical Biochemistry
Molecular Medicine
Abstract
Using the methodology of “click” chemistry, a series of conjugates of 3,5-bis(benzylidene)-1-(prop-2-yn)piperidin-4-ones with 4-alkyl-3-azidomethyl-2-ethoxy-2,5-dihydro-5H-1,2 oxaphosphol 2-oxides was synthesized. All newly obtained compounds 8–18 were characterized by 1H, 13C, 31P, 19F NMR and IR spectroscopy. The potential antitumor activity of the synthesized conjugates 8–18 was studied in terms of their ability to influence the viability of various cancer cell lines, including A549, SH-SY5Y, Hep-2, and HeLa. Compound 15, which contains two fluorine atoms in the benzene ring, was shown to be the most promising. The mechanism of the cytotoxic action of this conjugate is supposed to be associated with the ability to inhibit the glycolytic profile of transformed cells.
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E. Neganova M. et al. Synthesis and biological testing of 3,5-bis(arylidene)-4-piperidone conjugates with 2,5-dihydro-5H-1,2-oxaphospholenes // Bioorganic and Medicinal Chemistry Letters. 2022. Vol. 74. p. 128940.
GOST all authors (up to 50) Copy
E. Neganova M., Aleksandrova Y. R., Nikolaeva N. S., Brel V. K. Synthesis and biological testing of 3,5-bis(arylidene)-4-piperidone conjugates with 2,5-dihydro-5H-1,2-oxaphospholenes // Bioorganic and Medicinal Chemistry Letters. 2022. Vol. 74. p. 128940.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1016/j.bmcl.2022.128940
UR - https://doi.org/10.1016/j.bmcl.2022.128940
TI - Synthesis and biological testing of 3,5-bis(arylidene)-4-piperidone conjugates with 2,5-dihydro-5H-1,2-oxaphospholenes
T2 - Bioorganic and Medicinal Chemistry Letters
AU - E. Neganova, Margarita
AU - Aleksandrova, Yulia R.
AU - Nikolaeva, N S
AU - Brel, Valery K.
PY - 2022
DA - 2022/10/01
PB - Elsevier
SP - 128940
VL - 74
PMID - 35964843
SN - 0960-894X
SN - 1464-3405
ER -
BibTex
Cite this
BibTex (up to 50 authors) Copy
@article{2022_E. Neganova,
author = {Margarita E. Neganova and Yulia R. Aleksandrova and N S Nikolaeva and Valery K. Brel},
title = {Synthesis and biological testing of 3,5-bis(arylidene)-4-piperidone conjugates with 2,5-dihydro-5H-1,2-oxaphospholenes},
journal = {Bioorganic and Medicinal Chemistry Letters},
year = {2022},
volume = {74},
publisher = {Elsevier},
month = {oct},
url = {https://doi.org/10.1016/j.bmcl.2022.128940},
pages = {128940},
doi = {10.1016/j.bmcl.2022.128940}
}