Oxo/imido heterometathesis of N-sulfinylamines and carbonyl compounds catalyzed by silica-supported vanadium oxochloride
Pavel A Zhizhko
1, 2
,
Anton A Zhizhin
3
,
Dmitry N. Zarubin
3
,
N. A. Ustynyuk
3
,
Dmitry A Lemenovskii
2
,
Boris N Shelimov
4
,
Leonid Kustov
4
,
Publication type: Journal Article
Publication date: 2011-10-01
scimago Q1
wos Q1
SJR: 1.558
CiteScore: 10.9
Impact factor: 6.5
ISSN: 00219517, 10902694
Catalysis
Physical and Theoretical Chemistry
Abstract
Abstract A series of silica-supported vanadium oxo complexes has been prepared via water-free grafting VOCl3 onto the silica surface. The obtained materials have been characterized with Raman, diffuse reflectance FTIR (DRIFT) and UV–vis, 51V solid-state NMR and X-ray photoelectron spectroscopies, elemental analysis and N2 physisorption. The samples with a low vanadium loading (1–5%) have been found to be comprised primarily of the isolated tetrahedral d0 units ( SiO)V( O)Cl2, whereas the materials with a higher vanadium content are contaminated with a significant amount of d1 vanadium species. The silica-supported vanadium complexes act as heterogeneous catalysts for oxo/imido heterometathesis between N-sulfinylamines and carbonyl compounds affording imines and SO2. Grafting VOCl3 onto silica leads to a dramatic enhancement of its catalytic activity. A novel water-free express method for preparation of imines of wide range of aldehydes and some ketones has been developed. Noteworthy, this is the first example of transition metal mediated heterometathetical imidation of ketones.
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Total citations:
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Citations from 2024:
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(12%)
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GOST
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Zhizhko P. A. et al. Oxo/imido heterometathesis of N-sulfinylamines and carbonyl compounds catalyzed by silica-supported vanadium oxochloride // Journal of Catalysis. 2011. Vol. 283. No. 1. pp. 108-118.
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Zhizhko P. A., Zhizhin A. A., Zarubin D. N., Ustynyuk N. A., Lemenovskii D. A., Shelimov B. N., Kustov L., Kirichenko O. A., Kirakosyan G. Oxo/imido heterometathesis of N-sulfinylamines and carbonyl compounds catalyzed by silica-supported vanadium oxochloride // Journal of Catalysis. 2011. Vol. 283. No. 1. pp. 108-118.
Cite this
RIS
Copy
TY - JOUR
DO - 10.1016/j.jcat.2011.07.011
UR - https://linkinghub.elsevier.com/retrieve/pii/S0021951711002430
TI - Oxo/imido heterometathesis of N-sulfinylamines and carbonyl compounds catalyzed by silica-supported vanadium oxochloride
T2 - Journal of Catalysis
AU - Zhizhko, Pavel A
AU - Zhizhin, Anton A
AU - Zarubin, Dmitry N.
AU - Ustynyuk, N. A.
AU - Lemenovskii, Dmitry A
AU - Shelimov, Boris N
AU - Kustov, Leonid
AU - Kirichenko, Olga A.
AU - Kirakosyan, Gayane
PY - 2011
DA - 2011/10/01
PB - Elsevier
SP - 108-118
IS - 1
VL - 283
SN - 0021-9517
SN - 1090-2694
ER -
Cite this
BibTex (up to 50 authors)
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@article{2011_Zhizhko,
author = {Pavel A Zhizhko and Anton A Zhizhin and Dmitry N. Zarubin and N. A. Ustynyuk and Dmitry A Lemenovskii and Boris N Shelimov and Leonid Kustov and Olga A. Kirichenko and Gayane Kirakosyan},
title = {Oxo/imido heterometathesis of N-sulfinylamines and carbonyl compounds catalyzed by silica-supported vanadium oxochloride},
journal = {Journal of Catalysis},
year = {2011},
volume = {283},
publisher = {Elsevier},
month = {oct},
url = {https://linkinghub.elsevier.com/retrieve/pii/S0021951711002430},
number = {1},
pages = {108--118},
doi = {10.1016/j.jcat.2011.07.011}
}
Cite this
MLA
Copy
Zhizhko, Pavel A., et al. “Oxo/imido heterometathesis of N-sulfinylamines and carbonyl compounds catalyzed by silica-supported vanadium oxochloride.” Journal of Catalysis, vol. 283, no. 1, Oct. 2011, pp. 108-118. https://linkinghub.elsevier.com/retrieve/pii/S0021951711002430.