Access and in situ growth of phosphorene-precursor black phosphorus
Marianne Köpf
1
,
Nadine Eckstein
1
,
Daniela Pfister
1
,
Carolin Grotz
1
,
Ilona Krüger
1
,
Magnus Greiwe
1
,
Thomas M. Werge
2
,
Holger Kohlmann
3
,
Tom Nilges
1
Publication type: Journal Article
Publication date: 2014-11-01
scimago Q2
wos Q2
SJR: 0.424
CiteScore: 3.6
Impact factor: 2.0
ISSN: 00220248, 18735002
Materials Chemistry
Inorganic Chemistry
Condensed Matter Physics
Abstract
Single crystals of orthorhombic black phosphorus can be grown by a short way transport reaction from red phosphorus and Sn/SnI 4 as mineralization additive. Sizes of several millimeters can be realized with high crystal quality and purity, making a large area preparation of single or multilayer phosphorene possible. An in situ neutron diffraction study was performed addressing the formation of black phosphorus. Black phosphorus is formed directly via gas phase without the occurrence of any other intermediate phase. Crystal growth was initiated after cooling the starting materials down from elevated temperatures at 500 °C. • Large black phosphorus crystals were grown by a short way transport reaction. • In situ neutron diffraction affirms the formation of black P directly from gas phase. • Large crystals can be used as starting material for phosphorene synthesis.
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337
Total citations:
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Citations from 2025:
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(7.15%)
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Köpf M. et al. Access and in situ growth of phosphorene-precursor black phosphorus // Journal of Crystal Growth. 2014. Vol. 405. pp. 6-10.
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Köpf M., Eckstein N., Pfister D., Grotz C., Krüger I., Greiwe M., Werge T. M., Kohlmann H., Nilges T. Access and in situ growth of phosphorene-precursor black phosphorus // Journal of Crystal Growth. 2014. Vol. 405. pp. 6-10.
Cite this
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TY - JOUR
DO - 10.1016/j.jcrysgro.2014.07.029
UR - https://doi.org/10.1016/j.jcrysgro.2014.07.029
TI - Access and in situ growth of phosphorene-precursor black phosphorus
T2 - Journal of Crystal Growth
AU - Köpf, Marianne
AU - Eckstein, Nadine
AU - Pfister, Daniela
AU - Grotz, Carolin
AU - Krüger, Ilona
AU - Greiwe, Magnus
AU - Werge, Thomas M.
AU - Kohlmann, Holger
AU - Nilges, Tom
PY - 2014
DA - 2014/11/01
PB - Elsevier
SP - 6-10
VL - 405
SN - 0022-0248
SN - 1873-5002
ER -
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@article{2014_Köpf,
author = {Marianne Köpf and Nadine Eckstein and Daniela Pfister and Carolin Grotz and Ilona Krüger and Magnus Greiwe and Thomas M. Werge and Holger Kohlmann and Tom Nilges},
title = {Access and in situ growth of phosphorene-precursor black phosphorus},
journal = {Journal of Crystal Growth},
year = {2014},
volume = {405},
publisher = {Elsevier},
month = {nov},
url = {https://doi.org/10.1016/j.jcrysgro.2014.07.029},
pages = {6--10},
doi = {10.1016/j.jcrysgro.2014.07.029}
}