Synthesis, crystal and molecular structure of gold(I) thiophenolate with 4′-ferrocenyl[1,1′]biphenylisocyanides
Publication type: Journal Article
Publication date: 2010-01-01
scimago Q3
wos Q2
SJR: 0.385
CiteScore: 4.1
Impact factor: 2.4
ISSN: 0022328X, 18728561
Materials Chemistry
Organic Chemistry
Biochemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
Abstract The syntheses of ferrocenylbiphenylisocyanide gold(I) thiophenolato complexes are described. The preparative route starts from ferrocenylphenylbromide and proceeds in six steps to yield the desired gold(I) complexes, (thiophenolato)gold{(4′-ferrocenyl[1,1′]biphenyl-4-yl)isocyanide} ( 11 ) and (thiophenolato)gold{(4′-ferrocenyl-3,5-dimethyl[1,1′]biphenyl-4-yl)isocyanide} ( 12 ) in good yields. The synthetic pathways were developed as a first step toward realizing the goal of preparing metallomesogens based on ferrocenyl-polyphenylenes coordinated to gold(I) thiophenolates, in which long chain alkoxy groups are substituted para to sulfur on the phenyl ring. The crystal structures of (chloro)gold{(4 ′ -ferrocenyl[1,1′]biphenyl-4-yl)isocyanide} ( 9 ) and 12 are reported. Complex 9 crystallizes in the space group P 2 1 / c and 12 crystallizes in P 2 1 / n . Complexes 9 and 12 show short intermolecular Au–Au contacts of 3.3765(7) A and 3.3334(3) A, respectively.
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Dyadchenko V. P. et al. Synthesis, crystal and molecular structure of gold(I) thiophenolate with 4′-ferrocenyl[1,1′]biphenylisocyanides // Journal of Organometallic Chemistry. 2010. Vol. 695. No. 2. pp. 304-309.
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Dyadchenko V. P., Belov N. M., Lemenovskii D. A., Antipin M. Y., Lyssenko K. A., Bruce A. E., Bruce M. R. M. Synthesis, crystal and molecular structure of gold(I) thiophenolate with 4′-ferrocenyl[1,1′]biphenylisocyanides // Journal of Organometallic Chemistry. 2010. Vol. 695. No. 2. pp. 304-309.
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TY - JOUR
DO - 10.1016/j.jorganchem.2009.09.043
UR - https://linkinghub.elsevier.com/retrieve/pii/S0022328X09006469
TI - Synthesis, crystal and molecular structure of gold(I) thiophenolate with 4′-ferrocenyl[1,1′]biphenylisocyanides
T2 - Journal of Organometallic Chemistry
AU - Dyadchenko, V P
AU - Belov, N M
AU - Lemenovskii, D A
AU - Antipin, M. Yu.
AU - Lyssenko, Konstantin A.
AU - Bruce, Alice E.
AU - Bruce, Mitchell R. M.
PY - 2010
DA - 2010/01/01
PB - Elsevier
SP - 304-309
IS - 2
VL - 695
SN - 0022-328X
SN - 1872-8561
ER -
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@article{2010_Dyadchenko,
author = {V P Dyadchenko and N M Belov and D A Lemenovskii and M. Yu. Antipin and Konstantin A. Lyssenko and Alice E. Bruce and Mitchell R. M. Bruce},
title = {Synthesis, crystal and molecular structure of gold(I) thiophenolate with 4′-ferrocenyl[1,1′]biphenylisocyanides},
journal = {Journal of Organometallic Chemistry},
year = {2010},
volume = {695},
publisher = {Elsevier},
month = {jan},
url = {https://linkinghub.elsevier.com/retrieve/pii/S0022328X09006469},
number = {2},
pages = {304--309},
doi = {10.1016/j.jorganchem.2009.09.043}
}
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MLA
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Dyadchenko, V. P., et al. “Synthesis, crystal and molecular structure of gold(I) thiophenolate with 4′-ferrocenyl[1,1′]biphenylisocyanides.” Journal of Organometallic Chemistry, vol. 695, no. 2, Jan. 2010, pp. 304-309. https://linkinghub.elsevier.com/retrieve/pii/S0022328X09006469.