Synthesis of new carboranyl organosilicon derivatives – precursors for the preparation of hybrid organo-inorganic materials
Publication type: Journal Article
Publication date: 2020-12-01
scimago Q3
wos Q2
SJR: 0.385
CiteScore: 4.1
Impact factor: 2.4
ISSN: 0022328X, 18728561
Materials Chemistry
Organic Chemistry
Biochemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
• A series of new carboranyl organosilicon monomers have the potential to be used as high temperature oils, as building blocks in sol-gel processes and as a an additive in composites. • The versatile and easy preparation of the four polyhedral carboranyl derivatives are based on UV initiated hydrothiolation. • The compounds were isolated in good yields (65–95%) and characterized by 1 H, 11 B, 13 C and 29 Si NMR, IR spectroscopy, HRMS ESI and elemental microanalysis. • Assignment of 1 H and 13 C NMR spectra was made on the basis of 2D experiments of COSY, HMQC and HMBC. A series of new carboranyl organosilicon monomers have the potential to be used as high temperature oils, as building blocks in sol-gel processes and as an additive in composites. The versatile and easy preparation of the four polyhedral carboranyl derivatives are based on UV initiated hydrothiolation. The compounds were isolated in good yields (65–95%) and characterized by 1 H, 11 B, 13 C and 29 Si NMR, IR spectroscopy, HRMS ESI and elemental microanalysis. Assignment of 1 H and 13 C NMR spectra was made on the basis of 2D experiments of COSY, HMQC and HMBC.
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Minyaylo E. O. et al. Synthesis of new carboranyl organosilicon derivatives – precursors for the preparation of hybrid organo-inorganic materials // Journal of Organometallic Chemistry. 2020. Vol. 928. p. 121547.
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Minyaylo E. O., Anisimov A. A., Zaitsev A. Y., Ol'shevskaya V. A., Peregudov A. S., Kononova E., Shchegolikhina O. I., Muzafarov A. M., Möller M. Synthesis of new carboranyl organosilicon derivatives – precursors for the preparation of hybrid organo-inorganic materials // Journal of Organometallic Chemistry. 2020. Vol. 928. p. 121547.
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TY - JOUR
DO - 10.1016/j.jorganchem.2020.121547
UR - https://linkinghub.elsevier.com/retrieve/pii/S0022328X20304502
TI - Synthesis of new carboranyl organosilicon derivatives – precursors for the preparation of hybrid organo-inorganic materials
T2 - Journal of Organometallic Chemistry
AU - Minyaylo, Ekaterina O
AU - Anisimov, Anton A.
AU - Zaitsev, Andrei Yu.
AU - Ol'shevskaya, Valentina A.
AU - Peregudov, A. S.
AU - Kononova, E.G.
AU - Shchegolikhina, Olga I.
AU - Muzafarov, Aziz M.
AU - Möller, Martin
PY - 2020
DA - 2020/12/01
PB - Elsevier
SP - 121547
VL - 928
SN - 0022-328X
SN - 1872-8561
ER -
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@article{2020_Minyaylo,
author = {Ekaterina O Minyaylo and Anton A. Anisimov and Andrei Yu. Zaitsev and Valentina A. Ol'shevskaya and A. S. Peregudov and E.G. Kononova and Olga I. Shchegolikhina and Aziz M. Muzafarov and Martin Möller},
title = {Synthesis of new carboranyl organosilicon derivatives – precursors for the preparation of hybrid organo-inorganic materials},
journal = {Journal of Organometallic Chemistry},
year = {2020},
volume = {928},
publisher = {Elsevier},
month = {dec},
url = {https://linkinghub.elsevier.com/retrieve/pii/S0022328X20304502},
pages = {121547},
doi = {10.1016/j.jorganchem.2020.121547}
}