Synthesis and crystal structure of Mg2B24C, a new boron-rich boride related to “tetragonal boron I”
Тип публикации: Journal Article
Дата публикации: 2006-07-01
scimago Q2
wos Q1
white level БС2
SJR: 0.629
CiteScore: 6.8
Impact factor: 3.5
ISSN: 00224596, 1095726X
Materials Chemistry
Ceramics and Composites
Electronic, Optical and Magnetic Materials
Inorganic Chemistry
Physical and Theoretical Chemistry
Condensed Matter Physics
Краткое описание
Single crystals of Mg2B24C, a new boron-rich boridecarbide of magnesium, were synthesized as black needles and columns by reaction of the elements in Ta ampoules and BN crucibles at 1300 °C. The crystal structure was determined by X-ray diffraction (P-4n2, a = 8.9391 ( 13 ) A , c = 5.0745 ( 10 ) A , Z = 2 , 713 reflections, 64 variables, R 1 ( F ) = 0.0235 , w R 2 ( I ) = 0.0591 ). It is closely related to “tetragonal boron I” and can be described as a tetragonal rod packing of corner-linked B12 icosahedra with C and Mg atoms in the voids. Each B12 icosahedron has 2 B–C bonds and 10 exohedral bonds to other icosahedra, 2 within the rod and 4×2 to neighbouring rods. The isolated C atoms are 4-fold coordinated forming distorted tetrahedra. Mg is placed on two crystallographically independent positions within the three-dimensional B12C network. Mg2B24C is the first example for a compound related to “tetragonal boron I” with a stoichiometric composition.
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Adasch V. et al. Synthesis and crystal structure of Mg2B24C, a new boron-rich boride related to “tetragonal boron I” // Journal of Solid State Chemistry. 2006. Vol. 179. No. 7. pp. 2150-2157.
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Adasch V., Hess K., Ludwig T., Vojteer N., Hillebrecht H. Synthesis and crystal structure of Mg2B24C, a new boron-rich boride related to “tetragonal boron I” // Journal of Solid State Chemistry. 2006. Vol. 179. No. 7. pp. 2150-2157.
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TY - JOUR
DO - 10.1016/j.jssc.2006.04.021
UR - https://doi.org/10.1016/j.jssc.2006.04.021
TI - Synthesis and crystal structure of Mg2B24C, a new boron-rich boride related to “tetragonal boron I”
T2 - Journal of Solid State Chemistry
AU - Adasch, Volker
AU - Hess, Kai-Uwe
AU - Ludwig, Thilo
AU - Vojteer, Natascha
AU - Hillebrecht, H.
PY - 2006
DA - 2006/07/01
PB - Elsevier
SP - 2150-2157
IS - 7
VL - 179
SN - 0022-4596
SN - 1095-726X
ER -
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@article{2006_Adasch,
author = {Volker Adasch and Kai-Uwe Hess and Thilo Ludwig and Natascha Vojteer and H. Hillebrecht},
title = {Synthesis and crystal structure of Mg2B24C, a new boron-rich boride related to “tetragonal boron I”},
journal = {Journal of Solid State Chemistry},
year = {2006},
volume = {179},
publisher = {Elsevier},
month = {jul},
url = {https://doi.org/10.1016/j.jssc.2006.04.021},
number = {7},
pages = {2150--2157},
doi = {10.1016/j.jssc.2006.04.021}
}
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Adasch, Volker, et al. “Synthesis and crystal structure of Mg2B24C, a new boron-rich boride related to “tetragonal boron I”.” Journal of Solid State Chemistry, vol. 179, no. 7, Jul. 2006, pp. 2150-2157. https://doi.org/10.1016/j.jssc.2006.04.021.
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