Chlorotrimethylsilane-promoted synthesis of 1,2,4-triazolopyrimidines from 3,5-diamino-1,2,4-triazoles and pentane-2,4-diones
Publication type: Journal Article
Publication date: 2018-07-01
scimago Q3
wos Q3
SJR: 0.305
CiteScore: 3.0
Impact factor: 1.7
ISSN: 09599436, 1364551X
General Chemistry
Abstract
An efficient synthesis of 2-amino-1-R-[1,2,4]triazolo[1,5-a]-pyrimidinium or 3-amino-2-R-[1,2,4]triazolo[4,3-a]pyrimidi- nium chloride derivatives by heterocyclization of 3,5-diamino-1-R-1,2,4-triazoles (R = Alk or Ar) with pentane-2,4-diones was developed. The process is promoted by chlorotrimethyl- silane which plays the dual role of carbonyl-activating agent and water scavenger.
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Astakhov A. V. et al. Chlorotrimethylsilane-promoted synthesis of 1,2,4-triazolopyrimidines from 3,5-diamino-1,2,4-triazoles and pentane-2,4-diones // Mendeleev Communications. 2018. Vol. 28. No. 4. pp. 439-441.
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Astakhov A. V., Suponitsky K. Y., Chernyshev V. M. Chlorotrimethylsilane-promoted synthesis of 1,2,4-triazolopyrimidines from 3,5-diamino-1,2,4-triazoles and pentane-2,4-diones // Mendeleev Communications. 2018. Vol. 28. No. 4. pp. 439-441.
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TY - JOUR
DO - 10.1016/j.mencom.2018.07.034
UR - https://doi.org/10.1016/j.mencom.2018.07.034
TI - Chlorotrimethylsilane-promoted synthesis of 1,2,4-triazolopyrimidines from 3,5-diamino-1,2,4-triazoles and pentane-2,4-diones
T2 - Mendeleev Communications
AU - Astakhov, A. V.
AU - Suponitsky, Kyrill Yu.
AU - Chernyshev, Victor M.
PY - 2018
DA - 2018/07/01
PB - OOO Zhurnal "Mendeleevskie Soobshcheniya"
SP - 439-441
IS - 4
VL - 28
SN - 0959-9436
SN - 1364-551X
ER -
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@article{2018_Astakhov,
author = {A. V. Astakhov and Kyrill Yu. Suponitsky and Victor M. Chernyshev},
title = {Chlorotrimethylsilane-promoted synthesis of 1,2,4-triazolopyrimidines from 3,5-diamino-1,2,4-triazoles and pentane-2,4-diones},
journal = {Mendeleev Communications},
year = {2018},
volume = {28},
publisher = {OOO Zhurnal "Mendeleevskie Soobshcheniya"},
month = {jul},
url = {https://doi.org/10.1016/j.mencom.2018.07.034},
number = {4},
pages = {439--441},
doi = {10.1016/j.mencom.2018.07.034}
}
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MLA
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Astakhov, Alexander V., et al. “Chlorotrimethylsilane-promoted synthesis of 1,2,4-triazolopyrimidines from 3,5-diamino-1,2,4-triazoles and pentane-2,4-diones.” Mendeleev Communications, vol. 28, no. 4, Jul. 2018, pp. 439-441. https://doi.org/10.1016/j.mencom.2018.07.034.