Column chromatography separation of lanthanide(III) bisphthalocyaninate and phthalocyanine ligand
Publication type: Journal Article
Publication date: 2023-09-01
scimago Q3
wos Q3
SJR: 0.305
CiteScore: 3.0
Impact factor: 1.7
ISSN: 09599436, 1364551X
General Chemistry
Abstract
During the synthesis of double-decker f-metal phthalocyanine complexes Ln(Pc)2 free phthalocyanine ligands can be also formed, however, routine column chromatography is not effective for their separation. The preliminary reduction of the complexes with hydrazine hydrate affords the low mobile forms, which can be re-oxidized in the chromatography columns after the free ligand is eluted.
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Botnar A. A., Tikhomirova T. V., Vashurin A. Column chromatography separation of lanthanide(III) bisphthalocyaninate and phthalocyanine ligand // Mendeleev Communications. 2023. Vol. 33. No. 5. pp. 729-731.
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Botnar A. A., Tikhomirova T. V., Vashurin A. Column chromatography separation of lanthanide(III) bisphthalocyaninate and phthalocyanine ligand // Mendeleev Communications. 2023. Vol. 33. No. 5. pp. 729-731.
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TY - JOUR
DO - 10.1016/j.mencom.2023.09.044
UR - https://doi.org/10.1016/j.mencom.2023.09.044
TI - Column chromatography separation of lanthanide(III) bisphthalocyaninate and phthalocyanine ligand
T2 - Mendeleev Communications
AU - Botnar, A A
AU - Tikhomirova, Tatiana V
AU - Vashurin, Arthur
PY - 2023
DA - 2023/09/01
PB - OOO Zhurnal "Mendeleevskie Soobshcheniya"
SP - 729-731
IS - 5
VL - 33
SN - 0959-9436
SN - 1364-551X
ER -
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@article{2023_Botnar,
author = {A A Botnar and Tatiana V Tikhomirova and Arthur Vashurin},
title = {Column chromatography separation of lanthanide(III) bisphthalocyaninate and phthalocyanine ligand},
journal = {Mendeleev Communications},
year = {2023},
volume = {33},
publisher = {OOO Zhurnal "Mendeleevskie Soobshcheniya"},
month = {sep},
url = {https://doi.org/10.1016/j.mencom.2023.09.044},
number = {5},
pages = {729--731},
doi = {10.1016/j.mencom.2023.09.044}
}
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MLA
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Botnar, A. A., et al. “Column chromatography separation of lanthanide(III) bisphthalocyaninate and phthalocyanine ligand.” Mendeleev Communications, vol. 33, no. 5, Sep. 2023, pp. 729-731. https://doi.org/10.1016/j.mencom.2023.09.044.
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