Microporous and Mesoporous Materials

, том 116 , издание 1-3 , страницы 204-209

A new microporous MOF material based on Zn(II)-polycarboxylate coordination polymer synthesized with the aid of 1,6-diaminohexane as template

Тип публикации: Journal Article

Дата публикации: 2008-12-01

Elsevier

Microporous and Mesoporous Materials

scimago Q1

wos Q2

БС1

SJR: 1.003

CiteScore: 11

Impact factor: 4.7

ISSN: 13871811, 18733093

DOI: 10.1016/j.micromeso.2008.04.003

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General Chemistry

Condensed Matter Physics

General Materials Science

Mechanics of Materials

Краткое описание

A new microporous metal-organic framework (MOF) material ZBTEC-1 has been synthesized by designing infinite coordination polymer network formed between Zn(II) and 1,2,4,5-benzenetetracarboxylic acid (BTEC) under solvothermal conditions in the presence of 1,6-diaminohexane (DAH) as a single molecule template. Powder XRD data demonstrate that the ZBTEC-1 material has a new MOF structure. N 2 sorption studies indicated moderately good surface area (306 m 2 g −1 ) with large size micropores (average pore diameter ca . 0.7 nm) and very high pore volume (1.93 ccg −1 ). 13 C solid state MAS-NMR, FT-IR and UV–visible spectroscopic studies showed the presence of BTEC moieties in the framework. TEM and FE-SEM analysis indicated 30–60 nm diameter size microporous spherical particles for the ZBTEC-1 crystallites. This novel MOF material showed good hydrogen adsorption capacity at 77 K, indicating its potential application in hydrogen storage.

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Chandra D., Kasture M. W., Bhaumik A. A new microporous MOF material based on Zn(II)-polycarboxylate coordination polymer synthesized with the aid of 1,6-diaminohexane as template // Microporous and Mesoporous Materials. 2008. Vol. 116. No. 1-3. pp. 204-209.

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TY - JOUR

DO - 10.1016/j.micromeso.2008.04.003

UR - https://doi.org/10.1016/j.micromeso.2008.04.003

TI - A new microporous MOF material based on Zn(II)-polycarboxylate coordination polymer synthesized with the aid of 1,6-diaminohexane as template

T2 - Microporous and Mesoporous Materials

AU - Chandra, Debraj

AU - Kasture, Mahesh W

AU - Bhaumik, Asim

PY - 2008

DA - 2008/12/01

PB - Elsevier

SP - 204-209

IS - 1-3

VL - 116

SN - 1387-1811

SN - 1873-3093

ER -

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@article{2008_Chandra,

author = {Debraj Chandra and Mahesh W Kasture and Asim Bhaumik},

title = {A new microporous MOF material based on Zn(II)-polycarboxylate coordination polymer synthesized with the aid of 1,6-diaminohexane as template},

journal = {Microporous and Mesoporous Materials},

year = {2008},

volume = {116},

publisher = {Elsevier},

month = {dec},

url = {https://doi.org/10.1016/j.micromeso.2008.04.003},

number = {1-3},

pages = {204--209},

doi = {10.1016/j.micromeso.2008.04.003}

}

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Chandra, Debraj, et al. “A new microporous MOF material based on Zn(II)-polycarboxylate coordination polymer synthesized with the aid of 1,6-diaminohexane as template.” Microporous and Mesoporous Materials, vol. 116, no. 1-3, Dec. 2008, pp. 204-209. https://doi.org/10.1016/j.micromeso.2008.04.003.

Издатель

Elsevier

Журнал

Microporous and Mesoporous Materials

scimago Q1

wos Q2

БС1

SJR

1.003

CiteScore

Impact factor

4.7

ISSN

13871811 (Print)

18733093