Binuclear samarium(III) pivalates with chelating N-donors: Synthesis, structure, thermal behavior, magnetic and luminescent properties
I.G. Fomina
1
,
Zh V Dobrokhotova
1
,
А B Ilyukhin
1
,
G.G. Aleksandrov
1
,
V O Kazak
1
,
А Е Gehman
1
,
Y S Zavorotny
3
,
V.I. Gerasimova
3
,
V. M. Novotortsev
1
,
Publication type: Journal Article
Publication date: 2013-11-01
scimago Q3
wos Q2
SJR: 0.396
CiteScore: 4.9
Impact factor: 2.6
ISSN: 02775387, 18733719
Materials Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
Abstract The high-temperature solid-state desolvation under an inert atmosphere was studied for two new polymorphic complexes of the same composition (bath)2Sm2(piv)6·2EtOH (piv = (CH3)3CCO2−, bath = 4,7-diphenyl-1,10-phenanthroline), which differ in the structural functions of the bridging carboxylate anions. This resulted in the synthesis of new non-solvated pivalate (bath)2Sm2(piv)6. The complexes (bath)2Sm2(piv)6·2EtOH (two polymorphic modifications) and (bath)2Sm2(piv)6 were characterized by X-ray diffraction. The solid-state thermal decomposition of binuclear Sm(III) pivalates with heterocyclic chelating N-donors, such as 2,2′-bipyridyl (bpy), 1,10-phenanthroline (phen), and bath, was studied, the composition of the complexes in the gas phase was determined, and the magnetic and luminescent properties were analyzed.
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Fomina I. et al. Binuclear samarium(III) pivalates with chelating N-donors: Synthesis, structure, thermal behavior, magnetic and luminescent properties // Polyhedron. 2013. Vol. 65. pp. 152-160.
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Fomina I., Dobrokhotova Z. V., Ilyukhin А. B., Aleksandrov G., Kazak V. O., Gehman А. Е., Efimov N. N., Bogomyakov A. S., Zavorotny Y. S., Gerasimova V., Novotortsev V. M., Eremenko I. L. Binuclear samarium(III) pivalates with chelating N-donors: Synthesis, structure, thermal behavior, magnetic and luminescent properties // Polyhedron. 2013. Vol. 65. pp. 152-160.
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TY - JOUR
DO - 10.1016/j.poly.2013.08.017
UR - https://linkinghub.elsevier.com/retrieve/pii/S0277538713005792
TI - Binuclear samarium(III) pivalates with chelating N-donors: Synthesis, structure, thermal behavior, magnetic and luminescent properties
T2 - Polyhedron
AU - Fomina, I.G.
AU - Dobrokhotova, Zh V
AU - Ilyukhin, А B
AU - Aleksandrov, G.G.
AU - Kazak, V O
AU - Gehman, А Е
AU - Efimov, Nikolay N.
AU - Bogomyakov, Artem S
AU - Zavorotny, Y S
AU - Gerasimova, V.I.
AU - Novotortsev, V. M.
AU - Eremenko, Igor L.
PY - 2013
DA - 2013/11/01
PB - Elsevier
SP - 152-160
VL - 65
SN - 0277-5387
SN - 1873-3719
ER -
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BibTex (up to 50 authors)
Copy
@article{2013_Fomina,
author = {I.G. Fomina and Zh V Dobrokhotova and А B Ilyukhin and G.G. Aleksandrov and V O Kazak and А Е Gehman and Nikolay N. Efimov and Artem S Bogomyakov and Y S Zavorotny and V.I. Gerasimova and V. M. Novotortsev and Igor L. Eremenko},
title = {Binuclear samarium(III) pivalates with chelating N-donors: Synthesis, structure, thermal behavior, magnetic and luminescent properties},
journal = {Polyhedron},
year = {2013},
volume = {65},
publisher = {Elsevier},
month = {nov},
url = {https://linkinghub.elsevier.com/retrieve/pii/S0277538713005792},
pages = {152--160},
doi = {10.1016/j.poly.2013.08.017}
}