Tetrahedron

, том 64 , издание 22 , страницы 5055-5060

A simple and convenient synthesis of 4-methyl-3-nitro-2-trihalomethyl-2H-chromenes from N-unsubstituted imines of 2-hydroxyacetophenones and trichloro(trifluoro)ethylidene nitromethanes

Тип публикации: Journal Article

Дата публикации: 2008-05-01

Elsevier

Tetrahedron

scimago Q3

wos Q2

БС2

SJR: 0.426

CiteScore: 4.1

Impact factor: 2.2

ISSN: 00404020, 14645416

DOI: 10.1016/j.tet.2008.03.065

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Organic Chemistry

Drug Discovery

Biochemistry

Краткое описание

The reaction of N -unsubstituted imines of 2-hydroxyacetophenones with trichloro(trifluoro)ethylidene nitromethanes in the presence of DABCO proceeds via tandem oxa-Michael/aza-Henry additions (in dichloromethane) or aza-Michael addition (in benzene) to give 4-methyl-3-nitro-2-trichloro(trifluoro)methyl-2 H -chromenes or 1,1,1-trichloro(trifluoro)-3-nitro- N -[1-(2-hydroxyaryl)ethylidene]propan-2-amines, respectively.

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Korotaev V. Y. et al. A simple and convenient synthesis of 4-methyl-3-nitro-2-trihalomethyl-2H-chromenes from N-unsubstituted imines of 2-hydroxyacetophenones and trichloro(trifluoro)ethylidene nitromethanes // Tetrahedron. 2008. Vol. 64. No. 22. pp. 5055-5060.

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Korotaev V. Y., Sosnovskikh V. Y., Kutyashev I., Barkov A. V., Matochkina E. G., Kodess M. I. A simple and convenient synthesis of 4-methyl-3-nitro-2-trihalomethyl-2H-chromenes from N-unsubstituted imines of 2-hydroxyacetophenones and trichloro(trifluoro)ethylidene nitromethanes // Tetrahedron. 2008. Vol. 64. No. 22. pp. 5055-5060.

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TY - JOUR

DO - 10.1016/j.tet.2008.03.065

UR - https://doi.org/10.1016/j.tet.2008.03.065

TI - A simple and convenient synthesis of 4-methyl-3-nitro-2-trihalomethyl-2H-chromenes from N-unsubstituted imines of 2-hydroxyacetophenones and trichloro(trifluoro)ethylidene nitromethanes

T2 - Tetrahedron

AU - Korotaev, Vladislav Y

AU - Sosnovskikh, Vyacheslav Ya.

AU - Kutyashev, I.

AU - Barkov, Alexey V.

AU - Matochkina, Evgeniya G

AU - Kodess, Mikhail I.

PY - 2008

DA - 2008/05/01

PB - Elsevier

SP - 5055-5060

IS - 22

VL - 64

SN - 0040-4020

SN - 1464-5416

ER -

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@article{2008_Korotaev,

author = {Vladislav Y Korotaev and Vyacheslav Ya. Sosnovskikh and I. Kutyashev and Alexey V. Barkov and Evgeniya G Matochkina and Mikhail I. Kodess},

title = {A simple and convenient synthesis of 4-methyl-3-nitro-2-trihalomethyl-2H-chromenes from N-unsubstituted imines of 2-hydroxyacetophenones and trichloro(trifluoro)ethylidene nitromethanes},

journal = {Tetrahedron},

year = {2008},

volume = {64},

publisher = {Elsevier},

month = {may},

url = {https://doi.org/10.1016/j.tet.2008.03.065},

number = {22},

pages = {5055--5060},

doi = {10.1016/j.tet.2008.03.065}

}

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Korotaev, Vladislav Y., et al. “A simple and convenient synthesis of 4-methyl-3-nitro-2-trihalomethyl-2H-chromenes from N-unsubstituted imines of 2-hydroxyacetophenones and trichloro(trifluoro)ethylidene nitromethanes.” Tetrahedron, vol. 64, no. 22, May. 2008, pp. 5055-5060. https://doi.org/10.1016/j.tet.2008.03.065.