One-step synthesis of rccc- and rctt-diastereomers of novel calix[4]resorcinols based on a para-thiophosphorylated derivative of benzaldehyde
Irina R Knyazeva
1
,
Victoria I Sokolova
1
,
Margit Gruner
2
,
Wolf D. Habicher
2
,
B. Gabidullin
1
,
Michael A. Pudovik
1
Publication type: Journal Article
Publication date: 2013-07-01
scimago Q3
wos Q3
SJR: 0.334
CiteScore: 3.2
Impact factor: 1.5
ISSN: 00404039, 18733581
Organic Chemistry
Drug Discovery
Biochemistry
Abstract
Novel calix[4]resorcinols with four 2-thioxo-1,3,2-dioxaphosphorinane fragments included in aromatic substituents have been synthesized via a one-step condensation of resorcinol and its derivatives with a new para-thiophosphorylated benzaldehyde. It has been found that the diastereomeric ratio depends substantially on the reaction conditions, in particular, the solvents and catalysts used. The macrocyclic products obtained are rctt- and/or rccc-isomers, which were isolated and the structures determined by NMR and single crystal X-ray diffraction studies.
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Total citations:
21
Citations from 2025:
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(4.76%)
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GOST
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Knyazeva I. R. et al. One-step synthesis of rccc- and rctt-diastereomers of novel calix[4]resorcinols based on a para-thiophosphorylated derivative of benzaldehyde // Tetrahedron Letters. 2013. Vol. 54. No. 27. pp. 3538-3542.
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Knyazeva I. R., Sokolova V. I., Gruner M., Habicher W. D., Syakaev V. V., Khrizanforova V., Gabidullin B., Gubaidullin A. T., Budnikova Y. H., Burilov A. R., Pudovik M. A. One-step synthesis of rccc- and rctt-diastereomers of novel calix[4]resorcinols based on a para-thiophosphorylated derivative of benzaldehyde // Tetrahedron Letters. 2013. Vol. 54. No. 27. pp. 3538-3542.
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TY - JOUR
DO - 10.1016/j.tetlet.2013.04.114
UR - https://linkinghub.elsevier.com/retrieve/pii/S004040391300720X
TI - One-step synthesis of rccc- and rctt-diastereomers of novel calix[4]resorcinols based on a para-thiophosphorylated derivative of benzaldehyde
T2 - Tetrahedron Letters
AU - Knyazeva, Irina R
AU - Sokolova, Victoria I
AU - Gruner, Margit
AU - Habicher, Wolf D.
AU - Syakaev, Victor V.
AU - Khrizanforova, Vera
AU - Gabidullin, B.
AU - Gubaidullin, Aidar T.
AU - Budnikova, Yulia H.
AU - Burilov, Alexander R.
AU - Pudovik, Michael A.
PY - 2013
DA - 2013/07/01
PB - Elsevier
SP - 3538-3542
IS - 27
VL - 54
SN - 0040-4039
SN - 1873-3581
ER -
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BibTex (up to 50 authors)
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@article{2013_Knyazeva,
author = {Irina R Knyazeva and Victoria I Sokolova and Margit Gruner and Wolf D. Habicher and Victor V. Syakaev and Vera Khrizanforova and B. Gabidullin and Aidar T. Gubaidullin and Yulia H. Budnikova and Alexander R. Burilov and Michael A. Pudovik},
title = {One-step synthesis of rccc- and rctt-diastereomers of novel calix[4]resorcinols based on a para-thiophosphorylated derivative of benzaldehyde},
journal = {Tetrahedron Letters},
year = {2013},
volume = {54},
publisher = {Elsevier},
month = {jul},
url = {https://linkinghub.elsevier.com/retrieve/pii/S004040391300720X},
number = {27},
pages = {3538--3542},
doi = {10.1016/j.tetlet.2013.04.114}
}
Cite this
MLA
Copy
Knyazeva, Irina R., et al. “One-step synthesis of rccc- and rctt-diastereomers of novel calix[4]resorcinols based on a para-thiophosphorylated derivative of benzaldehyde.” Tetrahedron Letters, vol. 54, no. 27, Jul. 2013, pp. 3538-3542. https://linkinghub.elsevier.com/retrieve/pii/S004040391300720X.
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