Open Access

Ultrasonics Sonochemistry

, volume 24 , pages 230-237

Combined SANS and SAXS study of the action of ultrasound on the structure of amorphous zirconia gels

N N Gubanova ¹

A Ye Baranchikov ²

G. P. Kopitsa ¹

László Almásy ³

Borislav Angelov ⁴

Alexey Yapryntsev ²

L. Rosta ³

V. V. Ivanov ^{5, 6}

Hide authors affiliations Show authors affiliations: 6 affiliations

Petersburg Nuclear Physics Institute, Gatchina, Russia |

Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences Moscow Russia |

Institute for Solid State Physics and Optics, Wigner Research Centre for Physics, Hungarian Academy of Sciences, Hungary. |

⁴

Institute of Macromolecular Chemistry, Prague, Czech Republic |

⁵

Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences, Moscow, Russia |

⁶

National Research Tomsk State university, Tomsk, Russia |

Publication type: Journal Article

Publication date: 2015-05-01

Elsevier

Ultrasonics Sonochemistry

scimago Q1

wos Q1

SJR: 1.823

CiteScore: 17.7

Impact factor: 9.7

ISSN: 13504177, 18732828

DOI: 10.1016/j.ultsonch.2014.11.012

Copy DOI

PubMed ID: 25466600

Organic Chemistry

Inorganic Chemistry

Environmental Chemistry

Radiology Nuclear Medicine and imaging

Chemical Engineering (miscellaneous)

Acoustics and Ultrasonics

Abstract

In the present work, we have studied for the first time the combined effect of both sonication and precipitation pH on the structure of amorphous zirconia gels synthesized from zirconium(IV) propoxide. The techniques of small-angle neutron and X-ray scattering (SANS and SAXS) and low temperature nitrogen adsorption provided the integral data on the changes in the microstructure and mesostructure of these materials caused by ultrasonic (US) treatment. Amorphous ZrO2·xH2O synthesized under ultrasonic treatment was found to possess a very structured surface, characterized by the surface fractal dimension 2.9-3.0, compared to 2.3-2.5 for the non US-assisted synthesis, and it was also found to possess a higher specific surface area, while the sizes of the primary particles remain unchanged.

Found

3 citations

Baranchikov Alexander

PhD in Chemistry

400 publications, 5 202 citations, 274 reviews

h-index: 32

Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Research interests

Hydrothermal synthesis

Inorganic Chemistry

Low-temperature nitrogen adsorption

Rare-earth elements

Scanning electron microscopy

X-ray diffraction (XRD)

2 citations

Ivanov Vladimir

🥼

DSc in Chemistry, full member of the Russian Academy of Sciences

511 publications, 6 728 citations, 137 reviews

h-index: 37

Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Lomonosov Moscow State University

National Research University Higher School of Economics

Solid state chemistry

2 citations

Kottsov Sergei

🥼 🤝

38 publications, 194 citations, 5 reviews

h-index: 8

Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Lomonosov Moscow State University

Solid state chemistry

1 citation

Yapryntsev Alexey

🥼 🤝

PhD in Chemistry

82 publications, 727 citations

h-index: 17

Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

1 citation

Khodan A

44 publications, 907 citations, 1 review

h-index: 12

Tambov State University named after G.R. Derzhavin

A.N. Frumkin Institute of Physical Chemistry and Electrochemistry of the Russian Academy of Sciences

1 citation

Ivankov Oleksandr

117 publications, 1 599 citations

h-index: 23

Joint Institute for Nuclear Research

1 citation

Malkova Alena

40 publications, 350 citations

h-index: 10

Institute of Physiologically Active Compounds of the Russian Academy of Science

1 citation

Savastyanova Mariy

1 publication

h-index: 0

Institute of Technical Chemistry of the Ural Branch of the Russian Academy of Sciences

Perm Federal Research Center of the Ural Branch of the Russian Academy of Sciences

Research interests

Chemistry

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GOST |

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GOST Copy

Gubanova N. N. et al. Combined SANS and SAXS study of the action of ultrasound on the structure of amorphous zirconia gels // Ultrasonics Sonochemistry. 2015. Vol. 24. pp. 230-237.

GOST all authors (up to 50) Copy

Gubanova N. N., Baranchikov A. Y., Kopitsa G. P., Almásy L., Angelov B., Yapryntsev A., Rosta L., Ivanov V. V. Combined SANS and SAXS study of the action of ultrasound on the structure of amorphous zirconia gels // Ultrasonics Sonochemistry. 2015. Vol. 24. pp. 230-237.

RIS |

Cite this

RIS Copy

TY - JOUR

DO - 10.1016/j.ultsonch.2014.11.012

UR - https://linkinghub.elsevier.com/retrieve/pii/S1350417714003460

TI - Combined SANS and SAXS study of the action of ultrasound on the structure of amorphous zirconia gels

T2 - Ultrasonics Sonochemistry

AU - Gubanova, N N

AU - Baranchikov, A Ye

AU - Kopitsa, G. P.

AU - Almásy, László

AU - Angelov, Borislav

AU - Yapryntsev, Alexey

AU - Rosta, L.

AU - Ivanov, V. V.

PY - 2015

DA - 2015/05/01

PB - Elsevier

SP - 230-237

VL - 24

PMID - 25466600

SN - 1350-4177

SN - 1873-2828

ER -

BibTex

Cite this

BibTex (up to 50 authors) Copy

@article{2015_Gubanova,

author = {N N Gubanova and A Ye Baranchikov and G. P. Kopitsa and László Almásy and Borislav Angelov and Alexey Yapryntsev and L. Rosta and V. V. Ivanov},

title = {Combined SANS and SAXS study of the action of ultrasound on the structure of amorphous zirconia gels},

journal = {Ultrasonics Sonochemistry},

year = {2015},

volume = {24},

publisher = {Elsevier},

month = {may},

url = {https://linkinghub.elsevier.com/retrieve/pii/S1350417714003460},

pages = {230--237},

doi = {10.1016/j.ultsonch.2014.11.012}

}

Publisher

Elsevier

Journal

Ultrasonics Sonochemistry

scimago Q1

wos Q1

SJR

1.823

CiteScore

17.7

Impact factor

9.7

ISSN

13504177 (Print)

18732828 (Electronic)

Labs

Laboratory of synthesis of functional materials and processing of mineral raw materials

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