Liquid-Assisted Grinding Accelerating: Suzuki–Miyaura Reaction of Aryl Chlorides under High-Speed Ball-Milling Conditions
Publication type: Journal Article
Publication date: 2016-10-11
scimago Q2
wos Q1
SJR: 0.737
CiteScore: 6.1
Impact factor: 3.6
ISSN: 00223263, 15206904
PubMed ID:
27690440
Organic Chemistry
Abstract
The effect of liquid-assisted grinding has been studied using mechanical Suzuki-Miyaura reaction of aryl chlorides as the model reaction. Catalytic systems of Davephos and PCy3 are tested respectively showing strong influences from different liquids. Unexpected improvement of yield over 55% is observed using alcohols as additives, which is explained by in situ formed alkoxides and their participation in oxidative addition. Further expansion of substrates using Pd(OAc)2/PCy3/MeOH system gives desired products in good to high yields.
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Metrics
130
Total citations:
130
Citations from 2024:
37
(28.68%)
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MLA
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GOST
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Jiang Z. J. et al. Liquid-Assisted Grinding Accelerating: Suzuki–Miyaura Reaction of Aryl Chlorides under High-Speed Ball-Milling Conditions // Journal of Organic Chemistry. 2016. Vol. 81. No. 20. pp. 10049-10055.
GOST all authors (up to 50)
Copy
Jiang Z. J., Li Z., Yu J., Su W. Liquid-Assisted Grinding Accelerating: Suzuki–Miyaura Reaction of Aryl Chlorides under High-Speed Ball-Milling Conditions // Journal of Organic Chemistry. 2016. Vol. 81. No. 20. pp. 10049-10055.
Cite this
RIS
Copy
TY - JOUR
DO - 10.1021/acs.joc.6b01938
UR - https://doi.org/10.1021/acs.joc.6b01938
TI - Liquid-Assisted Grinding Accelerating: Suzuki–Miyaura Reaction of Aryl Chlorides under High-Speed Ball-Milling Conditions
T2 - Journal of Organic Chemistry
AU - Jiang, Zhi Jiang
AU - Li, Zhenhua
AU - Yu, Jingbo
AU - Su, Weike
PY - 2016
DA - 2016/10/11
PB - American Chemical Society (ACS)
SP - 10049-10055
IS - 20
VL - 81
PMID - 27690440
SN - 0022-3263
SN - 1520-6904
ER -
Cite this
BibTex (up to 50 authors)
Copy
@article{2016_Jiang,
author = {Zhi Jiang Jiang and Zhenhua Li and Jingbo Yu and Weike Su},
title = {Liquid-Assisted Grinding Accelerating: Suzuki–Miyaura Reaction of Aryl Chlorides under High-Speed Ball-Milling Conditions},
journal = {Journal of Organic Chemistry},
year = {2016},
volume = {81},
publisher = {American Chemical Society (ACS)},
month = {oct},
url = {https://doi.org/10.1021/acs.joc.6b01938},
number = {20},
pages = {10049--10055},
doi = {10.1021/acs.joc.6b01938}
}
Cite this
MLA
Copy
Jiang, Zhi Jiang, et al. “Liquid-Assisted Grinding Accelerating: Suzuki–Miyaura Reaction of Aryl Chlorides under High-Speed Ball-Milling Conditions.” Journal of Organic Chemistry, vol. 81, no. 20, Oct. 2016, pp. 10049-10055. https://doi.org/10.1021/acs.joc.6b01938.