Ni(3,5-CF3stb)2(Et2O): A “Super-Naked” Nickel Complex
Publication type: Journal Article
Publication date: 2024-07-11
scimago Q2
wos Q1
SJR: 0.676
CiteScore: 5.1
Impact factor: 2.9
ISSN: 02767333, 15206041
Abstract
Here, we report how the reduction of Ni(acac)2 in the presence of an electron-deficient stilbene (3,5-CF3stb (stb = trans-stilbene)) results in the formation of a heteroleptic 16-electron bis-(stilbene)Ni(0) complex supported by a labile Et2O ligand. The complex is highly reactive toward ligand exchange with even weakly coordinating species like arenes. While its reactivity in ethereal solvents is analogous to that of other tris-(stilbene)Ni(0), the ability to undergo ligand exchange with aromatic solvents permits access to currently inaccessible (stilbene)(η6-arene)Ni(0) complexes.
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Saeb R., Nöthling N., Cornella J. Ni(3,5-CF3stb)2(Et2O): A “Super-Naked” Nickel Complex // Organometallics. 2024. Vol. 43. No. 14. pp. 1511-1516.
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Saeb R., Nöthling N., Cornella J. Ni(3,5-CF3stb)2(Et2O): A “Super-Naked” Nickel Complex // Organometallics. 2024. Vol. 43. No. 14. pp. 1511-1516.
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TY - JOUR
DO - 10.1021/acs.organomet.4c00213
UR - https://pubs.acs.org/doi/10.1021/acs.organomet.4c00213
TI - Ni(3,5-CF3stb)2(Et2O): A “Super-Naked” Nickel Complex
T2 - Organometallics
AU - Saeb, Rakan
AU - Nöthling, Nils
AU - Cornella, Josep
PY - 2024
DA - 2024/07/11
PB - American Chemical Society (ACS)
SP - 1511-1516
IS - 14
VL - 43
SN - 0276-7333
SN - 1520-6041
ER -
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@article{2024_Saeb,
author = {Rakan Saeb and Nils Nöthling and Josep Cornella},
title = {Ni(3,5-CF3stb)2(Et2O): A “Super-Naked” Nickel Complex},
journal = {Organometallics},
year = {2024},
volume = {43},
publisher = {American Chemical Society (ACS)},
month = {jul},
url = {https://pubs.acs.org/doi/10.1021/acs.organomet.4c00213},
number = {14},
pages = {1511--1516},
doi = {10.1021/acs.organomet.4c00213}
}
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Saeb, Rakan, et al. “Ni(3,5-CF3stb)2(Et2O): A “Super-Naked” Nickel Complex.” Organometallics, vol. 43, no. 14, Jul. 2024, pp. 1511-1516. https://pubs.acs.org/doi/10.1021/acs.organomet.4c00213.