volume 22 issue 12 pages 4823-4827

Sustainable and Cost-Effective Suzuki–Miyaura Couplings toward the Key Biaryl Subunits of Arylex and Rinskor Active

Balaram S. Takale 1
Nicholas M Irvine 2
Abraham D Schuitman 2
Xiaoyong Li 2
Publication typeJournal Article
Publication date2020-06-10
scimago Q1
wos Q1
SJR1.235
CiteScore8.7
Impact factor5.0
ISSN15237060, 15237052
Organic Chemistry
Biochemistry
Physical and Theoretical Chemistry
Abstract
Challenging Suzuki-Miyaura cross couplings associated with novel crop protection active ingredients from Corteva Agriscience, Arylex and Rinskor, can be performed in water using parts per million (ppm) levels of a Pd catalyst. Each coupling required a distinct set of reaction conditions to achieve maximum selectivities and chemical yields. By way of comparison, this chemistry is not only performed under environmentally responsible aqueous micellar conditions, but also involves lowering loadings (3-5 times) of endangered palladium than used previously to attain a more sustainable process.
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GOST Copy
Takale B. S. et al. Sustainable and Cost-Effective Suzuki–Miyaura Couplings toward the Key Biaryl Subunits of Arylex and Rinskor Active // Organic Letters. 2020. Vol. 22. No. 12. pp. 4823-4827.
GOST all authors (up to 50) Copy
Takale B. S., Irvine N. M., Schuitman A. D., Li X., Lipshutz B. H. Sustainable and Cost-Effective Suzuki–Miyaura Couplings toward the Key Biaryl Subunits of Arylex and Rinskor Active // Organic Letters. 2020. Vol. 22. No. 12. pp. 4823-4827.
RIS |
Cite this
RIS Copy
TY - JOUR
DO - 10.1021/acs.orglett.0c01625
UR - https://doi.org/10.1021/acs.orglett.0c01625
TI - Sustainable and Cost-Effective Suzuki–Miyaura Couplings toward the Key Biaryl Subunits of Arylex and Rinskor Active
T2 - Organic Letters
AU - Takale, Balaram S.
AU - Irvine, Nicholas M
AU - Schuitman, Abraham D
AU - Li, Xiaoyong
AU - Lipshutz, Bruce H.
PY - 2020
DA - 2020/06/10
PB - American Chemical Society (ACS)
SP - 4823-4827
IS - 12
VL - 22
PMID - 32521158
SN - 1523-7060
SN - 1523-7052
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2020_Takale,
author = {Balaram S. Takale and Nicholas M Irvine and Abraham D Schuitman and Xiaoyong Li and Bruce H. Lipshutz},
title = {Sustainable and Cost-Effective Suzuki–Miyaura Couplings toward the Key Biaryl Subunits of Arylex and Rinskor Active},
journal = {Organic Letters},
year = {2020},
volume = {22},
publisher = {American Chemical Society (ACS)},
month = {jun},
url = {https://doi.org/10.1021/acs.orglett.0c01625},
number = {12},
pages = {4823--4827},
doi = {10.1021/acs.orglett.0c01625}
}
MLA
Cite this
MLA Copy
Takale, Balaram S., et al. “Sustainable and Cost-Effective Suzuki–Miyaura Couplings toward the Key Biaryl Subunits of Arylex and Rinskor Active.” Organic Letters, vol. 22, no. 12, Jun. 2020, pp. 4823-4827. https://doi.org/10.1021/acs.orglett.0c01625.