volume 24 issue 45 pages 8412-8416

trans-Trifluoromethyltetrafluorosulfanyl Chloride: Selective Synthesis and Reaction with Diazo Compounds

Publication typeJournal Article
Publication date2022-11-04
scimago Q1
wos Q1
SJR1.235
CiteScore8.7
Impact factor5.0
ISSN15237060, 15237052
Organic Chemistry
Biochemistry
Physical and Theoretical Chemistry
Abstract
trans-Trifluoromethyltetrafluorosulfanyl chloride (trans-CF3SF4Cl) is a unique reagent for the incorporation of the CF3SF4 group into organic compounds. However, CF3SF4Cl was prepared from hazardous reagents or formed as mixture of trans and cis isomers in low yield. Herein, a silver-promoted selective synthesis of trans-CF3SF4Cl under safe gas-reagent-free conditions is described. Furthermore, the synthetic application of trans-CF3SF4Cl is demonstrated through the new trifluoromethyltetrafluorosulfanylation of α-diazo carbonyl compounds.
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GOST |
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GOST Copy
Zhao X. et al. trans-Trifluoromethyltetrafluorosulfanyl Chloride: Selective Synthesis and Reaction with Diazo Compounds // Organic Letters. 2022. Vol. 24. No. 45. pp. 8412-8416.
GOST all authors (up to 50) Copy
Zhao X., Shou J. Y., Newton J. J., Qing F. trans-Trifluoromethyltetrafluorosulfanyl Chloride: Selective Synthesis and Reaction with Diazo Compounds // Organic Letters. 2022. Vol. 24. No. 45. pp. 8412-8416.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1021/acs.orglett.2c03540
UR - https://doi.org/10.1021/acs.orglett.2c03540
TI - trans-Trifluoromethyltetrafluorosulfanyl Chloride: Selective Synthesis and Reaction with Diazo Compounds
T2 - Organic Letters
AU - Zhao, Xin
AU - Shou, Jia Yi
AU - Newton, Josiah J
AU - Qing, Fengling
PY - 2022
DA - 2022/11/04
PB - American Chemical Society (ACS)
SP - 8412-8416
IS - 45
VL - 24
PMID - 36331806
SN - 1523-7060
SN - 1523-7052
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2022_Zhao,
author = {Xin Zhao and Jia Yi Shou and Josiah J Newton and Fengling Qing},
title = {trans-Trifluoromethyltetrafluorosulfanyl Chloride: Selective Synthesis and Reaction with Diazo Compounds},
journal = {Organic Letters},
year = {2022},
volume = {24},
publisher = {American Chemical Society (ACS)},
month = {nov},
url = {https://doi.org/10.1021/acs.orglett.2c03540},
number = {45},
pages = {8412--8416},
doi = {10.1021/acs.orglett.2c03540}
}
MLA
Cite this
MLA Copy
Zhao, Xin, et al. “trans-Trifluoromethyltetrafluorosulfanyl Chloride: Selective Synthesis and Reaction with Diazo Compounds.” Organic Letters, vol. 24, no. 45, Nov. 2022, pp. 8412-8416. https://doi.org/10.1021/acs.orglett.2c03540.