Journal of Organic Chemistry, volume 70, issue 22, pages 8739-8742

A Model Study toward the Total Synthesis of N-Deacetyllappaconitine

Douglass F Taber ¹

Jiang-Lin Liang ¹

Bei Chen ¹

Lisi Cai ¹

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Department of Chemistry and Biochemistry, University of Delaware, Newark, Delaware 19716 |

Publication type: Journal Article

Publication date: 2005-09-24

American Chemical Society (ACS)

Journal: Journal of Organic Chemistry

scimago Q2

wos Q1

SJR: 0.724

CiteScore: 6.2

Impact factor: 3.3

ISSN: 00223263, 15206904

DOI: 10.1021/jo051155y

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PubMed ID: 16238304

Organic Chemistry

Abstract

[reaction: see text] A model study leading to the preparation of the AEF rings of N-deacetyllappaconitine is described. The conjugate addition to the alpha-alkyl cyclohexenone 10 proceeded with high diastereocontrol. The Mannich cyclization of 16 to 4 was accomplished by heating with Rexyn-300 and Na(2)SO(4).

Found

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	2 4 6 8 10

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Publisher

American Chemical Society (ACS)

Journal

Journal of Organic Chemistry

scimago Q2

wos Q1

SJR

0.724

CiteScore

6.2

Impact factor

3.3

ISSN

00223263 (Print)

15206904 (Electronic)

A Model Study toward the Total Synthesis of N-Deacetyllappaconitine

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