Pressure-Induced Phase Transitions in Crystalline l - and dl -Cysteine
1
REC-008 Novosibirsk State University, Novosibirsk, Russia, Institute of Solid State Chemistry and Mechanochemistry SB RAS, Novosibirsk, Russia, Kirenskii Institute of Physics, Krasnoyarsk, Russia, Institute of Geology and Mineralogy SB RAS, Novosibirsk, Russia, and Institute of Organic Chemistry SB RAS, Novosibirsk, Russia
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Institute of Solid State Chemistry and Mechanochemistry of the Siberian Branch of the Russian Academy of Sciences
Kirensky Institute of Physics of the Siberian Branch of the Russian Academy of Sciences
Novosibirsk State University
V.S. Sobolev Institute of Geology and Mineralogy of the Siberian Branch of the Russian Academy of Sciences
N.N. Vorozhtsov Novosibirsk Institute of Organic Chemistry of the Siberian Branch of the Russian Academy of Sciences
Publication type: Journal Article
Publication date: 2008-07-01
scimago Q1
wos Q3
SJR: 0.742
CiteScore: 5.3
Impact factor: 2.9
ISSN: 15206106, 15205207, 10895647
PubMed ID:
18593144
Materials Chemistry
Surfaces, Coatings and Films
Physical and Theoretical Chemistry
Abstract
A series of extended reversible phase transitions at approximately 0.1, 1.5, 2.0, and approximately 5 GPa was observed for the first time in the crystals of dl-cysteine by Raman spectroscopy. These are the first examples of the phase transitions induced by increasing pressure in the racemic crystal of an amino acid. In the crystals of the orthorhombic l-cysteine, a sequence of reversible structural changes in the pressure range between 1.1 and 3 GPa could be observed by Raman spectroscopy, instead of a single sharp phase transition at 1.9 GPa reported previously in ( Moggach, et al. Acta Crystallogr. 2006, B62, 296- 309 ). The role of the movements of the side -CH 2SH groups and of the changes in the hydrogen-bonding type in dl- and l-cysteine during the phase transitions with increasing pressure is discussed and compared with that on cooling down to 3 K.
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Minkov V. S. et al. Pressure-Induced Phase Transitions in Crystalline l- and dl-Cysteine // Journal of Physical Chemistry B. 2008. Vol. 112. No. 30. pp. 8851-8854.
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Minkov V. S., Krylov A. A., Boldyreva E., Goryainov S. V., Bizyaev S. N., Vtyurin A. N. Pressure-Induced Phase Transitions in Crystalline l- and dl-Cysteine // Journal of Physical Chemistry B. 2008. Vol. 112. No. 30. pp. 8851-8854.
Cite this
RIS
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TY - JOUR
DO - 10.1021/jp8020276
UR - https://doi.org/10.1021/jp8020276
TI - Pressure-Induced Phase Transitions in Crystalline l- and dl-Cysteine
T2 - Journal of Physical Chemistry B
AU - Minkov, Vasil S
AU - Krylov, A. A.
AU - Boldyreva, Elena
AU - Goryainov, S. V.
AU - Bizyaev, Sergei N
AU - Vtyurin, Alexander N.
PY - 2008
DA - 2008/07/01
PB - American Chemical Society (ACS)
SP - 8851-8854
IS - 30
VL - 112
PMID - 18593144
SN - 1520-6106
SN - 1520-5207
SN - 1089-5647
ER -
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@article{2008_Minkov,
author = {Vasil S Minkov and A. A. Krylov and Elena Boldyreva and S. V. Goryainov and Sergei N Bizyaev and Alexander N. Vtyurin},
title = {Pressure-Induced Phase Transitions in Crystalline l- and dl-Cysteine},
journal = {Journal of Physical Chemistry B},
year = {2008},
volume = {112},
publisher = {American Chemical Society (ACS)},
month = {jul},
url = {https://doi.org/10.1021/jp8020276},
number = {30},
pages = {8851--8854},
doi = {10.1021/jp8020276}
}
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MLA
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Minkov, Vasil S., et al. “Pressure-Induced Phase Transitions in Crystalline l- and dl-Cysteine.” Journal of Physical Chemistry B, vol. 112, no. 30, Jul. 2008, pp. 8851-8854. https://doi.org/10.1021/jp8020276.
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