Fe(II)/Au(I) Relay Catalyzed Propargylisoxazole to Pyridine Isomerization: Access to 6-Halonicotinates
Тип публикации: Journal Article
Дата публикации: 2017-05-05
scimago Q2
wos Q1
БС1
SJR: 0.737
CiteScore: 6.1
Impact factor: 3.6
ISSN: 00223263, 15206904
PubMed ID:
28452217
Organic Chemistry
Краткое описание
An efficient synthesis of methyl nicotinates/6-halonicotinates by the domino isomerization of 4-propargyl/(3-halopropargyl)-5-methoxyisoxazoles under Fe(II)/Au(I) relay catalysis was developed. It was found that FeNTf2 is an effective catalyst for first step of the domino isomerization, transformation of isoxazole to 2H-azirine, which is compatible with Ph3PAuNTf2, catalyzing the second step.
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Galenko A. V. et al. Fe(II)/Au(I) Relay Catalyzed Propargylisoxazole to Pyridine Isomerization: Access to 6-Halonicotinates // Journal of Organic Chemistry. 2017. Vol. 82. No. 10. pp. 5367-5379.
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Galenko A. V., Shakirova F. M., Galenko E. E., Novikov M. S., Khlebnikov A. F. Fe(II)/Au(I) Relay Catalyzed Propargylisoxazole to Pyridine Isomerization: Access to 6-Halonicotinates // Journal of Organic Chemistry. 2017. Vol. 82. No. 10. pp. 5367-5379.
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TY - JOUR
DO - 10.1021/acs.joc.7b00736
UR - https://pubs.acs.org/doi/10.1021/acs.joc.7b00736
TI - Fe(II)/Au(I) Relay Catalyzed Propargylisoxazole to Pyridine Isomerization: Access to 6-Halonicotinates
T2 - Journal of Organic Chemistry
AU - Galenko, Alexey V
AU - Shakirova, Firuza M
AU - Galenko, Ekaterina E
AU - Novikov, Mikhail S.
AU - Khlebnikov, Alexander F
PY - 2017
DA - 2017/05/05
PB - American Chemical Society (ACS)
SP - 5367-5379
IS - 10
VL - 82
PMID - 28452217
SN - 0022-3263
SN - 1520-6904
ER -
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@article{2017_Galenko,
author = {Alexey V Galenko and Firuza M Shakirova and Ekaterina E Galenko and Mikhail S. Novikov and Alexander F Khlebnikov},
title = {Fe(II)/Au(I) Relay Catalyzed Propargylisoxazole to Pyridine Isomerization: Access to 6-Halonicotinates},
journal = {Journal of Organic Chemistry},
year = {2017},
volume = {82},
publisher = {American Chemical Society (ACS)},
month = {may},
url = {https://pubs.acs.org/doi/10.1021/acs.joc.7b00736},
number = {10},
pages = {5367--5379},
doi = {10.1021/acs.joc.7b00736}
}
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MLA
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Galenko, Alexey V., et al. “Fe(II)/Au(I) Relay Catalyzed Propargylisoxazole to Pyridine Isomerization: Access to 6-Halonicotinates.” Journal of Organic Chemistry, vol. 82, no. 10, May. 2017, pp. 5367-5379. https://pubs.acs.org/doi/10.1021/acs.joc.7b00736.
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