Journal of Organic Chemistry

, том 83 , издание 1 , страницы 478-483

Copper-Catalyzed Coupling of Acyl Chlorides with gem-Difluorinated Organozinc Reagents via Acyl Dithiocarbamates

Тип публикации: Journal Article

Дата публикации: 2017-12-11

American Chemical Society (ACS)

Journal of Organic Chemistry

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SJR: 0.737

CiteScore: 6.1

Impact factor: 3.6

ISSN: 00223263, 15206904

DOI: 10.1021/acs.joc.7b02598

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PubMed ID: 29178788

Organic Chemistry

Краткое описание

A cross-coupling of acyl chlorides with gem-difluorinated organozinc reagents affording difluorinated ketones is described. In the reaction, acyl chlorides are first treated with potassium dithiocarbamate to generate S-acyl dithiocarbamates, which couple with organozincs in the presence of a copper(I) catalyst.

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Котовщиков Юрий

27 публикаций, 393 цитирования, 31 рецензия

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Московский государственный университет имени М.В. Ломоносова

1 цитирование

Дильман Александр

д.х.н., ч.-к., Российская академия наук

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Институт органической химии им. Н.Д. Зелинского РАН

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Органическая химия

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Ashirbaev S. S. et al. Copper-Catalyzed Coupling of Acyl Chlorides with gem-Difluorinated Organozinc Reagents via Acyl Dithiocarbamates // Journal of Organic Chemistry. 2017. Vol. 83. No. 1. pp. 478-483.

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Ashirbaev S. S., Levin V. V., Struchkova M. I., Dilman A. D. Copper-Catalyzed Coupling of Acyl Chlorides with gem-Difluorinated Organozinc Reagents via Acyl Dithiocarbamates // Journal of Organic Chemistry. 2017. Vol. 83. No. 1. pp. 478-483.

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TY - JOUR

DO - 10.1021/acs.joc.7b02598

UR - https://doi.org/10.1021/acs.joc.7b02598

TI - Copper-Catalyzed Coupling of Acyl Chlorides with gem-Difluorinated Organozinc Reagents via Acyl Dithiocarbamates

T2 - Journal of Organic Chemistry

AU - Ashirbaev, Salavat S

AU - Levin, Vitalij V

AU - Struchkova, Marina I.

AU - Dilman, Alexander D

PY - 2017

DA - 2017/12/11

PB - American Chemical Society (ACS)

SP - 478-483

IS - 1

VL - 83

PMID - 29178788

SN - 0022-3263

SN - 1520-6904

ER -

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@article{2017_Ashirbaev,

author = {Salavat S Ashirbaev and Vitalij V Levin and Marina I. Struchkova and Alexander D Dilman},

title = {Copper-Catalyzed Coupling of Acyl Chlorides with gem-Difluorinated Organozinc Reagents via Acyl Dithiocarbamates},

journal = {Journal of Organic Chemistry},

year = {2017},

volume = {83},

publisher = {American Chemical Society (ACS)},

month = {dec},

url = {https://doi.org/10.1021/acs.joc.7b02598},

number = {1},

pages = {478--483},

doi = {10.1021/acs.joc.7b02598}

}

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Ashirbaev, Salavat S., et al. “Copper-Catalyzed Coupling of Acyl Chlorides with gem-Difluorinated Organozinc Reagents via Acyl Dithiocarbamates.” Journal of Organic Chemistry, vol. 83, no. 1, Dec. 2017, pp. 478-483. https://doi.org/10.1021/acs.joc.7b02598.