American Chemical Society (ACS)
Journal of Organic Chemistry
,  volume 83 ,  issue 24 ,  pages 15493-15498

Photochemical Preparation of 1,2-Dihydro-3H-indazol-3-ones in Aqueous Solvent at Room Temperature

Publication type: Journal Article
Publication date: 2018-11-23
American Chemical Society (ACS)
scimago Q2
wos Q1
SJR: 0.737
CiteScore: 6.1
Impact factor: 3.6
ISSN: 00223263, 15206904
Organic Chemistry
Abstract
o-Nitrosobenzaldehyde is a reactive intermediate useful in the synthesis of nitrogen heterocycles. Previous strategies for using o-nitrosobenzaldehyde involve its isolation via chromatography and/or formation under harsh conditions. Herein, this intermediate was photochemically generated in situ from o-nitrobenzyl alcohols in a mild, efficient manner for the construction of 1,2-dihydro-3 H-indazol-3-ones using an aqueous solvent at room temperature. This convenient reaction offers several advantages over reported methods. The commercially available photoreactor employed 3 × 18 W bulbs outputting broad emission above 365 nm.
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GOST Copy
Zhu J. S. et al. Photochemical Preparation of 1,2-Dihydro-3H-indazol-3-ones in Aqueous Solvent at Room Temperature // Journal of Organic Chemistry. 2018. Vol. 83. No. 24. pp. 15493-15498.
GOST all authors (up to 50) Copy
Zhu J. S., Kraemer N., Li C. J., Haddadin M., Kurth M. J. Photochemical Preparation of 1,2-Dihydro-3H-indazol-3-ones in Aqueous Solvent at Room Temperature // Journal of Organic Chemistry. 2018. Vol. 83. No. 24. pp. 15493-15498.
RIS |
Cite this
RIS Copy
TY - JOUR
DO - 10.1021/acs.joc.8b02356
UR - https://doi.org/10.1021/acs.joc.8b02356
TI - Photochemical Preparation of 1,2-Dihydro-3H-indazol-3-ones in Aqueous Solvent at Room Temperature
T2 - Journal of Organic Chemistry
AU - Zhu, Jie S
AU - Kraemer, Niklas
AU - Li, Clarabella J
AU - Haddadin, Makhluf
AU - Kurth, Mark J.
PY - 2018
DA - 2018/11/23
PB - American Chemical Society (ACS)
SP - 15493-15498
IS - 24
VL - 83
PMID - 30468072
SN - 0022-3263
SN - 1520-6904
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2018_Zhu,
author = {Jie S Zhu and Niklas Kraemer and Clarabella J Li and Makhluf Haddadin and Mark J. Kurth},
title = {Photochemical Preparation of 1,2-Dihydro-3H-indazol-3-ones in Aqueous Solvent at Room Temperature},
journal = {Journal of Organic Chemistry},
year = {2018},
volume = {83},
publisher = {American Chemical Society (ACS)},
month = {nov},
url = {https://doi.org/10.1021/acs.joc.8b02356},
number = {24},
pages = {15493--15498},
doi = {10.1021/acs.joc.8b02356}
}
MLA
Cite this
MLA Copy
Zhu, Jie S., et al. “Photochemical Preparation of 1,2-Dihydro-3H-indazol-3-ones in Aqueous Solvent at Room Temperature.” Journal of Organic Chemistry, vol. 83, no. 24, Nov. 2018, pp. 15493-15498. https://doi.org/10.1021/acs.joc.8b02356.