NMR and EPR Characterization of Functionalized Nanodiamonds
Тип публикации: Journal Article
Дата публикации: 2015-05-21
scimago Q1
wos Q3
БС1
SJR: 0.914
CiteScore: 6.2
Impact factor: 3.2
ISSN: 19327447, 19327455
Surfaces, Coatings and Films
Electronic, Optical and Magnetic Materials
Physical and Theoretical Chemistry
General Energy
Краткое описание
We investigated the potential of solid-state NMR using magic angle spinning (MAS) with and without dynamic nuclear polarization (DNP) and electron paramagnetic resonance (EPR) for the characterization of functionalized nanodiamonds (NDs). We showed that conventional 1H, 31P, and 13C solid-state NMR spectra allow differentiating in a straightforward way NDs from commercial sources and custom-made NDs bearing aromatic or aliphatic phosphonate moieties at their surface. Besides, the short nuclear relaxation times prove the close proximity between the endogenous paramagnetic centers of NDs and the grafted organic moieties. EPR spectra confirmed the presence of these paramagnetic centers in functionalized NDs, which are centered on dangling bonds as well as a few N0 defects, corresponding to the substitution of carbon atoms by nitrogen ones. Hyperfine sublevel correlation spectroscopy indicates that the N0 paramagnetic centers are mostly located in the disordered shell of NDs. Preliminary DNP-enhanced NMR expe...
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Presti C. et al. NMR and EPR Characterization of Functionalized Nanodiamonds // Journal of Physical Chemistry C. 2015. Vol. 119. No. 22. pp. 12408-12422.
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Presti C., Thankamony A. S. L., Alauzun J. G., Mutin P., Carnevale D., Lion C., Vezin H., Laurencin D., Lafon O. NMR and EPR Characterization of Functionalized Nanodiamonds // Journal of Physical Chemistry C. 2015. Vol. 119. No. 22. pp. 12408-12422.
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TY - JOUR
DO - 10.1021/acs.jpcc.5b02171
UR - https://doi.org/10.1021/acs.jpcc.5b02171
TI - NMR and EPR Characterization of Functionalized Nanodiamonds
T2 - Journal of Physical Chemistry C
AU - Presti, Charlene
AU - Thankamony, Aany S Lilly
AU - Alauzun, Johan G.
AU - Mutin, P.Hubert
AU - Carnevale, Diego
AU - Lion, Cedric
AU - Vezin, Hervé
AU - Laurencin, Danielle
AU - Lafon, Olivier
PY - 2015
DA - 2015/05/21
PB - American Chemical Society (ACS)
SP - 12408-12422
IS - 22
VL - 119
SN - 1932-7447
SN - 1932-7455
ER -
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@article{2015_Presti,
author = {Charlene Presti and Aany S Lilly Thankamony and Johan G. Alauzun and P.Hubert Mutin and Diego Carnevale and Cedric Lion and Hervé Vezin and Danielle Laurencin and Olivier Lafon},
title = {NMR and EPR Characterization of Functionalized Nanodiamonds},
journal = {Journal of Physical Chemistry C},
year = {2015},
volume = {119},
publisher = {American Chemical Society (ACS)},
month = {may},
url = {https://doi.org/10.1021/acs.jpcc.5b02171},
number = {22},
pages = {12408--12422},
doi = {10.1021/acs.jpcc.5b02171}
}
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Presti, Charlene, et al. “NMR and EPR Characterization of Functionalized Nanodiamonds.” Journal of Physical Chemistry C, vol. 119, no. 22, May. 2015, pp. 12408-12422. https://doi.org/10.1021/acs.jpcc.5b02171.