Ultrahigh-Molecular-Weight Triblock Copolymers via Inverse Miniemulsion Photoiniferter Polymerization
Тип публикации: Journal Article
Дата публикации: 2024-04-17
scimago Q1
wos Q1
БС1
SJR: 1.352
CiteScore: 9
Impact factor: 5.2
ISSN: 00249297, 15205835
Materials Chemistry
Organic Chemistry
Inorganic Chemistry
Polymers and Plastics
Краткое описание
We report the successful synthesis of ultrahigh-molecular-weight (UHMW, 106–107 g/mol) ABA triblock copolymers through photoiniferter polymerization using solution and inverse miniemulsion conditions. The photoiniferter process was first employed in homogeneous aqueous media to prepare telechelic UHMW poly(N,N-dimethylacrylamide). The effect of the R-group of the iniferter (ZC(═S)SR) on the polymerization control and rate was investigated. The chain-end fidelity of the resulting polymers was verified through sequential chain extensions in solution. Various iniferters were investigated for their hydrolytic stability and partitioning between aqueous and organic phases. Relying on these learnings, the photoiniferter synthesis of UHMW ABA triblock copolymers was achieved under inverse miniemulsion conditions, and the approach was expanded in monomer scope to incorporate 3-acrylamidophenylboronic acid units to impart stimuli-responsive behavior.
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Lott M. E. et al. Ultrahigh-Molecular-Weight Triblock Copolymers via Inverse Miniemulsion Photoiniferter Polymerization // Macromolecules. 2024. Vol. 57. No. 9. pp. 4007-4015.
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Lott M. E., Trachsel L., Schué E., Davidson C. L. G., Olson S R. A., Pedro D. I., Pedro D. I., Chang F., Hong Y., Sawyer W. H., Sumerlin B. S. Ultrahigh-Molecular-Weight Triblock Copolymers via Inverse Miniemulsion Photoiniferter Polymerization // Macromolecules. 2024. Vol. 57. No. 9. pp. 4007-4015.
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TY - JOUR
DO - 10.1021/acs.macromol.4c00366
UR - https://pubs.acs.org/doi/10.1021/acs.macromol.4c00366
TI - Ultrahigh-Molecular-Weight Triblock Copolymers via Inverse Miniemulsion Photoiniferter Polymerization
T2 - Macromolecules
AU - Lott, Megan E
AU - Trachsel, Lucca
AU - Schué, Emmanuelle
AU - Davidson, Cullen L G
AU - Olson S, Rebecca A.
AU - Pedro, Diego I
AU - Pedro, D. I.
AU - Chang, Frank
AU - Hong, Ye
AU - Sawyer, W H
AU - Sumerlin, Brent S.
PY - 2024
DA - 2024/04/17
PB - American Chemical Society (ACS)
SP - 4007-4015
IS - 9
VL - 57
SN - 0024-9297
SN - 1520-5835
ER -
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@article{2024_Lott,
author = {Megan E Lott and Lucca Trachsel and Emmanuelle Schué and Cullen L G Davidson and Rebecca A. Olson S and Diego I Pedro and D. I. Pedro and Frank Chang and Ye Hong and W H Sawyer and Brent S. Sumerlin},
title = {Ultrahigh-Molecular-Weight Triblock Copolymers via Inverse Miniemulsion Photoiniferter Polymerization},
journal = {Macromolecules},
year = {2024},
volume = {57},
publisher = {American Chemical Society (ACS)},
month = {apr},
url = {https://pubs.acs.org/doi/10.1021/acs.macromol.4c00366},
number = {9},
pages = {4007--4015},
doi = {10.1021/acs.macromol.4c00366}
}
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MLA
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Lott, Megan E., et al. “Ultrahigh-Molecular-Weight Triblock Copolymers via Inverse Miniemulsion Photoiniferter Polymerization.” Macromolecules, vol. 57, no. 9, Apr. 2024, pp. 4007-4015. https://pubs.acs.org/doi/10.1021/acs.macromol.4c00366.