volume 22 issue 6 pages 2365-2370

Total Synthesis of Micrococcin P1 through Scalable Thiazole Forming Reactions of Cysteine Derivatives and Nitriles

Mitchell P Christy 1
Trevor Johnson 1
Clare D Mcnerlin 2
John Woodard 2
Andrew T. Nelson 3, 4
Bryant Lim 2
Tiffany L Hamilton 2
Kaitlyn M Freiberg 2
Dionicio Siegel 2
Publication typeJournal Article
Publication date2020-03-05
scimago Q1
wos Q1
SJR1.235
CiteScore8.7
Impact factor5.0
ISSN15237060, 15237052
Organic Chemistry
Biochemistry
Physical and Theoretical Chemistry
Abstract
Thiopeptides are a class of natural products with untapped therapeutic potential. To expand the methods available for the scaled production of these antibiotics, we report the laboratory synthesis of micrococcin P1 showcasing thiazole forming reactions of cysteine derivatives and nitriles followed by oxidation. In most instances, this thiazole forming sequence does not require chromatography and proved scalable. Using this approach, 199 mg of micrococcin P1 was generated in a single synthetic sequence.
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GOST |
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GOST Copy
Christy M. P. et al. Total Synthesis of Micrococcin P1 through Scalable Thiazole Forming Reactions of Cysteine Derivatives and Nitriles // Organic Letters. 2020. Vol. 22. No. 6. pp. 2365-2370.
GOST all authors (up to 50) Copy
Christy M. P., Johnson T., Mcnerlin C. D., Woodard J., Nelson A. T., Lim B., Hamilton T. L., Freiberg K. M., Siegel D. Total Synthesis of Micrococcin P1 through Scalable Thiazole Forming Reactions of Cysteine Derivatives and Nitriles // Organic Letters. 2020. Vol. 22. No. 6. pp. 2365-2370.
RIS |
Cite this
RIS Copy
TY - JOUR
DO - 10.1021/acs.orglett.0c00202
UR - https://doi.org/10.1021/acs.orglett.0c00202
TI - Total Synthesis of Micrococcin P1 through Scalable Thiazole Forming Reactions of Cysteine Derivatives and Nitriles
T2 - Organic Letters
AU - Christy, Mitchell P
AU - Johnson, Trevor
AU - Mcnerlin, Clare D
AU - Woodard, John
AU - Nelson, Andrew T.
AU - Lim, Bryant
AU - Hamilton, Tiffany L
AU - Freiberg, Kaitlyn M
AU - Siegel, Dionicio
PY - 2020
DA - 2020/03/05
PB - American Chemical Society (ACS)
SP - 2365-2370
IS - 6
VL - 22
PMID - 32134277
SN - 1523-7060
SN - 1523-7052
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2020_Christy,
author = {Mitchell P Christy and Trevor Johnson and Clare D Mcnerlin and John Woodard and Andrew T. Nelson and Bryant Lim and Tiffany L Hamilton and Kaitlyn M Freiberg and Dionicio Siegel},
title = {Total Synthesis of Micrococcin P1 through Scalable Thiazole Forming Reactions of Cysteine Derivatives and Nitriles},
journal = {Organic Letters},
year = {2020},
volume = {22},
publisher = {American Chemical Society (ACS)},
month = {mar},
url = {https://doi.org/10.1021/acs.orglett.0c00202},
number = {6},
pages = {2365--2370},
doi = {10.1021/acs.orglett.0c00202}
}
MLA
Cite this
MLA Copy
Christy, Mitchell P., et al. “Total Synthesis of Micrococcin P1 through Scalable Thiazole Forming Reactions of Cysteine Derivatives and Nitriles.” Organic Letters, vol. 22, no. 6, Mar. 2020, pp. 2365-2370. https://doi.org/10.1021/acs.orglett.0c00202.