Sodium Hypophosphite as a Bulk and Environmentally Friendly Reducing Agent in the Reductive Amination
Тип публикации: Journal Article
Дата публикации: 2022-10-14
scimago Q1
wos Q1
БС1
SJR: 1.235
CiteScore: 8.7
Impact factor: 5.0
ISSN: 15237060, 15237052
PubMed ID:
36240121
Organic Chemistry
Biochemistry
Physical and Theoretical Chemistry
Краткое описание
NaH2PO2 was found to promote reductive amination. Being nontoxic, stable, environmentally benign, and available in bulk amounts, this reducing agent showed a powerful potential to compete with classical reductants applied in the target process. An E factor of 1 was achieved for the substrate scope. Different carbonyl compounds reacted with amines under the developed conditions. The reaction demonstrated a great compatibility with a wide range of functional groups. Reaction conditions were scaled up to 200-fold.
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Kliuev F. S. et al. Sodium Hypophosphite as a Bulk and Environmentally Friendly Reducing Agent in the Reductive Amination // Organic Letters. 2022. Vol. 24. No. 42. pp. 7717-7721.
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Kliuev F. S., Kuznetsov A., Afanasyev O. I., Runikhina S. A., Kuchuk E., Podyacheva E., Tsygankov A. A., Chusov D. Sodium Hypophosphite as a Bulk and Environmentally Friendly Reducing Agent in the Reductive Amination // Organic Letters. 2022. Vol. 24. No. 42. pp. 7717-7721.
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TY - JOUR
DO - 10.1021/acs.orglett.2c02807
UR - https://pubs.acs.org/doi/10.1021/acs.orglett.2c02807
TI - Sodium Hypophosphite as a Bulk and Environmentally Friendly Reducing Agent in the Reductive Amination
T2 - Organic Letters
AU - Kliuev, Fedor S
AU - Kuznetsov, Anton
AU - Afanasyev, Oleg I
AU - Runikhina, Sofiya A
AU - Kuchuk, Ekaterina
AU - Podyacheva, Evgeniya
AU - Tsygankov, Alexey A
AU - Chusov, Denis
PY - 2022
DA - 2022/10/14
PB - American Chemical Society (ACS)
SP - 7717-7721
IS - 42
VL - 24
PMID - 36240121
SN - 1523-7060
SN - 1523-7052
ER -
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@article{2022_Kliuev,
author = {Fedor S Kliuev and Anton Kuznetsov and Oleg I Afanasyev and Sofiya A Runikhina and Ekaterina Kuchuk and Evgeniya Podyacheva and Alexey A Tsygankov and Denis Chusov},
title = {Sodium Hypophosphite as a Bulk and Environmentally Friendly Reducing Agent in the Reductive Amination},
journal = {Organic Letters},
year = {2022},
volume = {24},
publisher = {American Chemical Society (ACS)},
month = {oct},
url = {https://pubs.acs.org/doi/10.1021/acs.orglett.2c02807},
number = {42},
pages = {7717--7721},
doi = {10.1021/acs.orglett.2c02807}
}
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MLA
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Kliuev, Fedor S., et al. “Sodium Hypophosphite as a Bulk and Environmentally Friendly Reducing Agent in the Reductive Amination.” Organic Letters, vol. 24, no. 42, Oct. 2022, pp. 7717-7721. https://pubs.acs.org/doi/10.1021/acs.orglett.2c02807.
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