Sodium Hypophosphite as a Bulk and Environmentally Friendly Reducing Agent in the Reductive Amination
Fedor S Kliuev
1, 2
,
Anton Kuznetsov
3
,
Oleg I Afanasyev
1
,
Sofiya A Runikhina
1
,
Ekaterina Kuchuk
1
,
Evgeniya Podyacheva
1, 2
,
Denis Chusov
1, 4
3
Moscow South-Eastern School named after V.I. Chuikov (Moscow Chemical Lyceum), Tamozhenniy proezd 4, Moscow 111033, Russian Federation
|
Publication type: Journal Article
Publication date: 2022-10-14
scimago Q1
wos Q1
SJR: 1.235
CiteScore: 8.7
Impact factor: 5.0
ISSN: 15237060, 15237052
PubMed ID:
36240121
Organic Chemistry
Biochemistry
Physical and Theoretical Chemistry
Abstract
NaH2PO2 was found to promote reductive amination. Being nontoxic, stable, environmentally benign, and available in bulk amounts, this reducing agent showed a powerful potential to compete with classical reductants applied in the target process. An E factor of 1 was achieved for the substrate scope. Different carbonyl compounds reacted with amines under the developed conditions. The reaction demonstrated a great compatibility with a wide range of functional groups. Reaction conditions were scaled up to 200-fold.
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18
Total citations:
18
Citations from 2024:
13
(76.47%)
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GOST
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Kliuev F. S. et al. Sodium Hypophosphite as a Bulk and Environmentally Friendly Reducing Agent in the Reductive Amination // Organic Letters. 2022. Vol. 24. No. 42. pp. 7717-7721.
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Kliuev F. S., Kuznetsov A., Afanasyev O. I., Runikhina S. A., Kuchuk E., Podyacheva E., Tsygankov A. A., Chusov D. Sodium Hypophosphite as a Bulk and Environmentally Friendly Reducing Agent in the Reductive Amination // Organic Letters. 2022. Vol. 24. No. 42. pp. 7717-7721.
Cite this
RIS
Copy
TY - JOUR
DO - 10.1021/acs.orglett.2c02807
UR - https://pubs.acs.org/doi/10.1021/acs.orglett.2c02807
TI - Sodium Hypophosphite as a Bulk and Environmentally Friendly Reducing Agent in the Reductive Amination
T2 - Organic Letters
AU - Kliuev, Fedor S
AU - Kuznetsov, Anton
AU - Afanasyev, Oleg I
AU - Runikhina, Sofiya A
AU - Kuchuk, Ekaterina
AU - Podyacheva, Evgeniya
AU - Tsygankov, Alexey A
AU - Chusov, Denis
PY - 2022
DA - 2022/10/14
PB - American Chemical Society (ACS)
SP - 7717-7721
IS - 42
VL - 24
PMID - 36240121
SN - 1523-7060
SN - 1523-7052
ER -
Cite this
BibTex (up to 50 authors)
Copy
@article{2022_Kliuev,
author = {Fedor S Kliuev and Anton Kuznetsov and Oleg I Afanasyev and Sofiya A Runikhina and Ekaterina Kuchuk and Evgeniya Podyacheva and Alexey A Tsygankov and Denis Chusov},
title = {Sodium Hypophosphite as a Bulk and Environmentally Friendly Reducing Agent in the Reductive Amination},
journal = {Organic Letters},
year = {2022},
volume = {24},
publisher = {American Chemical Society (ACS)},
month = {oct},
url = {https://pubs.acs.org/doi/10.1021/acs.orglett.2c02807},
number = {42},
pages = {7717--7721},
doi = {10.1021/acs.orglett.2c02807}
}
Cite this
MLA
Copy
Kliuev, Fedor S., et al. “Sodium Hypophosphite as a Bulk and Environmentally Friendly Reducing Agent in the Reductive Amination.” Organic Letters, vol. 24, no. 42, Oct. 2022, pp. 7717-7721. https://pubs.acs.org/doi/10.1021/acs.orglett.2c02807.