Organic Letters

, том 19 , издание 20 , страницы 5641-5644

A Bench-Stable, Single-Component Precatalyst for Silyl–Heck Reactions

Тип публикации: Journal Article

Дата публикации: 2017-09-29

American Chemical Society (ACS)

Organic Letters

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SJR: 1.007

CiteScore: 7.7

Impact factor: 4.7

ISSN: 15237060, 15237052

DOI: 10.1021/acs.orglett.7b02807

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PubMed ID: 28960083

Organic Chemistry

Biochemistry

Physical and Theoretical Chemistry

Краткое описание

Studies of the silyl-Heck reaction aimed at identifying active palladium complexes have revealed a new species that is formed in situ. This complex has been identified as the palladium iodide dimer, [(JessePhos)PdI2]2, which has been found to be a competent single-component precatalyst for the silyl-Heck reaction. This complex is easily prepared and is temperature, moisture, and air stable. Additionally, this precatalyst provides higher activity and greater reproducibility compared to previous systems.

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Krause S. B. et al. A Bench-Stable, Single-Component Precatalyst for Silyl–Heck Reactions // Organic Letters. 2017. Vol. 19. No. 20. pp. 5641-5644.

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Krause S. B., Mcatee J. R., Yap G. P. A., WATSON D. P. A Bench-Stable, Single-Component Precatalyst for Silyl–Heck Reactions // Organic Letters. 2017. Vol. 19. No. 20. pp. 5641-5644.

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TY - JOUR

DO - 10.1021/acs.orglett.7b02807

UR - https://doi.org/10.1021/acs.orglett.7b02807

TI - A Bench-Stable, Single-Component Precatalyst for Silyl–Heck Reactions

T2 - Organic Letters

AU - Krause, Sarah B

AU - Mcatee, Jesse R

AU - Yap, Glenn P. A.

AU - WATSON, DONALD P.

PY - 2017

DA - 2017/09/29

PB - American Chemical Society (ACS)

SP - 5641-5644

IS - 20

VL - 19

PMID - 28960083

SN - 1523-7060

SN - 1523-7052

ER -

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@article{2017_Krause,

author = {Sarah B Krause and Jesse R Mcatee and Glenn P. A. Yap and DONALD P. WATSON},

title = {A Bench-Stable, Single-Component Precatalyst for Silyl–Heck Reactions},

journal = {Organic Letters},

year = {2017},

volume = {19},

publisher = {American Chemical Society (ACS)},

month = {sep},

url = {https://doi.org/10.1021/acs.orglett.7b02807},

number = {20},

pages = {5641--5644},

doi = {10.1021/acs.orglett.7b02807}

}

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Krause, Sarah B., et al. “A Bench-Stable, Single-Component Precatalyst for Silyl–Heck Reactions.” Organic Letters, vol. 19, no. 20, Sep. 2017, pp. 5641-5644. https://doi.org/10.1021/acs.orglett.7b02807.

Издатель

American Chemical Society (ACS)

Журнал

Organic Letters

SCImago Q1

Tоп 10% SCImago

WOS Q1

БС1