Organic Letters

, том 20 , издание 24 , страницы 7856-7859

Atom- and Step-Economical Ruthenium-Catalyzed Synthesis of Esters from Aldehydes or Ketones and Carboxylic Acids.

Тип публикации: Journal Article

Дата публикации: 2018-12-07

American Chemical Society (ACS)

Organic Letters

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SJR: 1.235

CiteScore: 8.7

Impact factor: 5

ISSN: 15237060, 15237052

DOI: 10.1021/acs.orglett.8b03375

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PubMed ID: 30525672

Organic Chemistry

Biochemistry

Physical and Theoretical Chemistry

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We developed a ruthenium-catalyzed reductive ester synthesis from aldehydes or ketones and carboxylic acids using carbon monoxide as a deoxygenative agent. Multiple factors influencing the outcome of the reaction were investigated. Best results were obtained for commercially available and inexpensive benzene ruthenium chloride; as low as 0.5 mol % of the catalyst is sufficient for efficient reaction. Competitive studies demonstrated that the presence of even 1000 equiv of alcohol in the reaction mixture does not lead to the corresponding ester, which clearly indicates that the process is not a simple reductive esterification but a novel type of Ru-catalyzed redox process.

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Runikhina S. A. et al. Atom- and Step-Economical Ruthenium-Catalyzed Synthesis of Esters from Aldehydes or Ketones and Carboxylic Acids. // Organic Letters. 2018. Vol. 20. No. 24. pp. 7856-7859.

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Runikhina S. A., Usanov D. A., Chizhov A. O., Chusov D. Atom- and Step-Economical Ruthenium-Catalyzed Synthesis of Esters from Aldehydes or Ketones and Carboxylic Acids. // Organic Letters. 2018. Vol. 20. No. 24. pp. 7856-7859.

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TY - JOUR

DO - 10.1021/acs.orglett.8b03375

UR - https://doi.org/10.1021/acs.orglett.8b03375

TI - Atom- and Step-Economical Ruthenium-Catalyzed Synthesis of Esters from Aldehydes or Ketones and Carboxylic Acids.

T2 - Organic Letters

AU - Runikhina, Sofiya A

AU - Usanov, Dmitry A.

AU - Chizhov, A. O.

AU - Chusov, Denis

PY - 2018

DA - 2018/12/07

PB - American Chemical Society (ACS)

SP - 7856-7859

IS - 24

VL - 20

PMID - 30525672

SN - 1523-7060

SN - 1523-7052

ER -

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@article{2018_Runikhina,

author = {Sofiya A Runikhina and Dmitry A. Usanov and A. O. Chizhov and Denis Chusov},

title = {Atom- and Step-Economical Ruthenium-Catalyzed Synthesis of Esters from Aldehydes or Ketones and Carboxylic Acids.},

journal = {Organic Letters},

year = {2018},

volume = {20},

publisher = {American Chemical Society (ACS)},

month = {dec},

url = {https://doi.org/10.1021/acs.orglett.8b03375},

number = {24},

pages = {7856--7859},

doi = {10.1021/acs.orglett.8b03375}

}

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Runikhina, Sofiya A., et al. “Atom- and Step-Economical Ruthenium-Catalyzed Synthesis of Esters from Aldehydes or Ketones and Carboxylic Acids..” Organic Letters, vol. 20, no. 24, Dec. 2018, pp. 7856-7859. https://doi.org/10.1021/acs.orglett.8b03375.