volume 20 issue 24 pages 7856-7859

Atom- and Step-Economical Ruthenium-Catalyzed Synthesis of Esters from Aldehydes or Ketones and Carboxylic Acids.

Publication typeJournal Article
Publication date2018-12-07
scimago Q1
wos Q1
SJR1.235
CiteScore8.7
Impact factor5.0
ISSN15237060, 15237052
Organic Chemistry
Biochemistry
Physical and Theoretical Chemistry
Abstract
We developed a ruthenium-catalyzed reductive ester synthesis from aldehydes or ketones and carboxylic acids using carbon monoxide as a deoxygenative agent. Multiple factors influencing the outcome of the reaction were investigated. Best results were obtained for commercially available and inexpensive benzene ruthenium chloride; as low as 0.5 mol % of the catalyst is sufficient for efficient reaction. Competitive studies demonstrated that the presence of even 1000 equiv of alcohol in the reaction mixture does not lead to the corresponding ester, which clearly indicates that the process is not a simple reductive esterification but a novel type of Ru-catalyzed redox process.
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GOST Copy
Runikhina S. A. et al. Atom- and Step-Economical Ruthenium-Catalyzed Synthesis of Esters from Aldehydes or Ketones and Carboxylic Acids. // Organic Letters. 2018. Vol. 20. No. 24. pp. 7856-7859.
GOST all authors (up to 50) Copy
Runikhina S. A., Usanov D. A., Chizhov A. O., Chusov D. Atom- and Step-Economical Ruthenium-Catalyzed Synthesis of Esters from Aldehydes or Ketones and Carboxylic Acids. // Organic Letters. 2018. Vol. 20. No. 24. pp. 7856-7859.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1021/acs.orglett.8b03375
UR - https://doi.org/10.1021/acs.orglett.8b03375
TI - Atom- and Step-Economical Ruthenium-Catalyzed Synthesis of Esters from Aldehydes or Ketones and Carboxylic Acids.
T2 - Organic Letters
AU - Runikhina, Sofiya A
AU - Usanov, Dmitry A.
AU - Chizhov, A. O.
AU - Chusov, Denis
PY - 2018
DA - 2018/12/07
PB - American Chemical Society (ACS)
SP - 7856-7859
IS - 24
VL - 20
PMID - 30525672
SN - 1523-7060
SN - 1523-7052
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2018_Runikhina,
author = {Sofiya A Runikhina and Dmitry A. Usanov and A. O. Chizhov and Denis Chusov},
title = {Atom- and Step-Economical Ruthenium-Catalyzed Synthesis of Esters from Aldehydes or Ketones and Carboxylic Acids.},
journal = {Organic Letters},
year = {2018},
volume = {20},
publisher = {American Chemical Society (ACS)},
month = {dec},
url = {https://doi.org/10.1021/acs.orglett.8b03375},
number = {24},
pages = {7856--7859},
doi = {10.1021/acs.orglett.8b03375}
}
MLA
Cite this
MLA Copy
Runikhina, Sofiya A., et al. “Atom- and Step-Economical Ruthenium-Catalyzed Synthesis of Esters from Aldehydes or Ketones and Carboxylic Acids..” Organic Letters, vol. 20, no. 24, Dec. 2018, pp. 7856-7859. https://doi.org/10.1021/acs.orglett.8b03375.
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