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Thermogravimetric Determination of the Kinetics of Petroleum Needle Coke Formation by Decantoil Thermolysis

Kondrasheva N.K., Rudko V.A., Ancheyta J.
Тип документаJournal Article
Дата публикации2020-11-05
Название журналаACS Omega
ИздательAmerican Chemical Society
Квартиль по SCImagoQ1
Квартиль по Web of ScienceQ2
Импакт-фактор 20214.13
ISSN24701343
General Chemistry
General Chemical Engineering
Краткое описание
This work presents the results of thermogravimetric analysis of decantoil. The microstructure of the extracted petroleum coke during the thermolysis of decantoil in an inert nitrogen atmosphere at 1000 °C was studied by scanning electron microscopy and interpreted as acicular. The model free kinetic approach based on Friedman’s isoconversion method was used to calculate the kinetic characteristics of decantoil thermolysis-activation energy and pre-exponential factor. The individual hydrocarbon composition of decantoil was determined by gas chromatography mass spectrometry, which was used to determine the activation energy of evaporation of its fractions. The total energy spent on the chemical reactions of cracking and thermopolycondensation was determined when the degree of decantoil conversion was changed from 0.1 to 0.9.
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1. Kondrasheva N. K., Rudko V. A., Ancheyta J. Thermogravimetric Determination of the Kinetics of Petroleum Needle Coke Formation by Decantoil Thermolysis // ACS Omega. 2020. Т. 5. № 45. С. 29570–29576.
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TY - JOUR

DO - 10.1021/acsomega.0c04552

UR - http://dx.doi.org/10.1021/acsomega.0c04552

TI - Thermogravimetric Determination of the Kinetics of Petroleum Needle Coke Formation by Decantoil Thermolysis

T2 - ACS Omega

AU - Kondrasheva, Natalia K.

AU - Rudko, Viacheslav A.

AU - Ancheyta, Jorge

PY - 2020

DA - 2020/11/05

PB - American Chemical Society (ACS)

SP - 29570-29576

IS - 45

VL - 5

SN - 2470-1343

SN - 2470-1343

ER -

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@article{Kondrasheva_2020,

doi = {10.1021/acsomega.0c04552},

url = {https://doi.org/10.1021%2Facsomega.0c04552},

year = 2020,

month = {nov},

publisher = {American Chemical Society ({ACS})},

volume = {5},

number = {45},

pages = {29570--29576},

author = {Natalia K. Kondrasheva and Viacheslav A. Rudko and Jorge Ancheyta},

title = {Thermogravimetric Determination of the Kinetics of Petroleum Needle Coke Formation by Decantoil Thermolysis},

journal = {{ACS} Omega}

}

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Kondrasheva, Natalia K., et al. “Thermogravimetric Determination of the Kinetics of Petroleum Needle Coke Formation by Decantoil Thermolysis.” ACS Omega, vol. 5, no. 45, Nov. 2020, pp. 29570–76. Crossref, https://doi.org/10.1021/acsomega.0c04552.