Open Access
Quantitative Determination of Trace Heavy Metals and Selected Rock-Forming Elements in Porous Carbon Materials by the X-ray Fluorescence Method
Publication type: Journal Article
Publication date: 2021-09-15
scimago Q1
wos Q2
SJR: 0.773
CiteScore: 7.1
Impact factor: 4.3
ISSN: 24701343
PubMed ID:
34604641
General Chemistry
General Chemical Engineering
Abstract
A new X-ray fluorescence (XRF) method is proposed for sample preparation and impurity quantification for elements heavier than sodium in carbon materials. The analysis is suitable for various materials including amorphous ones, such as petroleum cokes, with an impurity content higher than 0.01%. We compared a new method with the regular additive method to measure impurities in electrode graphite and petroleum coke. The XRF-based method provides the same sensitivity and accuracy and much greater reproducibility of the analysis results for variations in the sample mass, its density, and coverage by exciting X-ray radiation. The method does not require changes in the instrument software and is easily implemented on commercial analytical equipment.
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Metrics
21
Total citations:
21
Citations from 2024:
12
(57%)
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MLA
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GOST
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Povarov V. G. et al. Quantitative Determination of Trace Heavy Metals and Selected Rock-Forming Elements in Porous Carbon Materials by the X-ray Fluorescence Method // ACS Omega. 2021. Vol. 6. No. 38. pp. 24595-24601.
GOST all authors (up to 50)
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Povarov V. G., Kopylova T. N., Sinyakova M. A., Rudko V. A. Quantitative Determination of Trace Heavy Metals and Selected Rock-Forming Elements in Porous Carbon Materials by the X-ray Fluorescence Method // ACS Omega. 2021. Vol. 6. No. 38. pp. 24595-24601.
Cite this
RIS
Copy
TY - JOUR
DO - 10.1021/acsomega.1c03217
UR - https://doi.org/10.1021/acsomega.1c03217
TI - Quantitative Determination of Trace Heavy Metals and Selected Rock-Forming Elements in Porous Carbon Materials by the X-ray Fluorescence Method
T2 - ACS Omega
AU - Povarov, Vladimir G
AU - Kopylova, Tatyana N
AU - Sinyakova, Maria A
AU - Rudko, Viacheslav A
PY - 2021
DA - 2021/09/15
PB - American Chemical Society (ACS)
SP - 24595-24601
IS - 38
VL - 6
PMID - 34604641
SN - 2470-1343
ER -
Cite this
BibTex (up to 50 authors)
Copy
@article{2021_Povarov,
author = {Vladimir G Povarov and Tatyana N Kopylova and Maria A Sinyakova and Viacheslav A Rudko},
title = {Quantitative Determination of Trace Heavy Metals and Selected Rock-Forming Elements in Porous Carbon Materials by the X-ray Fluorescence Method},
journal = {ACS Omega},
year = {2021},
volume = {6},
publisher = {American Chemical Society (ACS)},
month = {sep},
url = {https://doi.org/10.1021/acsomega.1c03217},
number = {38},
pages = {24595--24601},
doi = {10.1021/acsomega.1c03217}
}
Cite this
MLA
Copy
Povarov, Vladimir G., et al. “Quantitative Determination of Trace Heavy Metals and Selected Rock-Forming Elements in Porous Carbon Materials by the X-ray Fluorescence Method.” ACS Omega, vol. 6, no. 38, Sep. 2021, pp. 24595-24601. https://doi.org/10.1021/acsomega.1c03217.