Applying Green Metrics to Eco-Friendly Synthesis of Sulfur-Substituted Conjugated Dienes Based on Atom-Economic Hydrothiolation
Тип публикации: Journal Article
Дата публикации: 2019-04-30
scimago Q1
wos Q1
БС1
SJR: 1.623
CiteScore: 12.5
Impact factor: 7.3
ISSN: 21680485
General Chemistry
General Chemical Engineering
Environmental Chemistry
Renewable Energy, Sustainability and the Environment
Краткое описание
An efficient two-step procedure to get synthetically useful sulfur-functionalized dienes is evaluated. The overall transformation can be classified as an atom-economic hydrothiolation of alkynes followed by elimination of water at the dehydration step. Taking the alkynes hydrofunctionalization reaction as a representative example, critical analysis from the point of view of quantitative green metrics was carried out and key stumbling blocks in the area of atom-economic transformations were discussed. Ecological acceptability of the whole process was assessed by thorough examination of the yields and careful adjustment of the synthetic conditions, considering the opportunities for waste minimization. Careful optimization of the reaction conditions was followed by selection of environmentally friendly protocols for accessing pure product. Green metrics of synthetic procedures as well as different isolation techniques (column chromatography, dry column chromatography, extraction, and distillation) were compa...
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Degtyareva E. S., Borkovskaya E. V., Ananikov V. P. Applying Green Metrics to Eco-Friendly Synthesis of Sulfur-Substituted Conjugated Dienes Based on Atom-Economic Hydrothiolation // ACS Sustainable Chemistry and Engineering. 2019. Vol. 7. No. 10. pp. 9680-9689.
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Degtyareva E. S., Borkovskaya E. V., Ananikov V. P. Applying Green Metrics to Eco-Friendly Synthesis of Sulfur-Substituted Conjugated Dienes Based on Atom-Economic Hydrothiolation // ACS Sustainable Chemistry and Engineering. 2019. Vol. 7. No. 10. pp. 9680-9689.
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TY - JOUR
DO - 10.1021/acssuschemeng.9b01405
UR - https://doi.org/10.1021/acssuschemeng.9b01405
TI - Applying Green Metrics to Eco-Friendly Synthesis of Sulfur-Substituted Conjugated Dienes Based on Atom-Economic Hydrothiolation
T2 - ACS Sustainable Chemistry and Engineering
AU - Degtyareva, Evgeniya S
AU - Borkovskaya, Evgeniya V
AU - Ananikov, Valentine P
PY - 2019
DA - 2019/04/30
PB - American Chemical Society (ACS)
SP - 9680-9689
IS - 10
VL - 7
SN - 2168-0485
ER -
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@article{2019_Degtyareva,
author = {Evgeniya S Degtyareva and Evgeniya V Borkovskaya and Valentine P Ananikov},
title = {Applying Green Metrics to Eco-Friendly Synthesis of Sulfur-Substituted Conjugated Dienes Based on Atom-Economic Hydrothiolation},
journal = {ACS Sustainable Chemistry and Engineering},
year = {2019},
volume = {7},
publisher = {American Chemical Society (ACS)},
month = {apr},
url = {https://doi.org/10.1021/acssuschemeng.9b01405},
number = {10},
pages = {9680--9689},
doi = {10.1021/acssuschemeng.9b01405}
}
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MLA
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Degtyareva, Evgeniya S., et al. “Applying Green Metrics to Eco-Friendly Synthesis of Sulfur-Substituted Conjugated Dienes Based on Atom-Economic Hydrothiolation.” ACS Sustainable Chemistry and Engineering, vol. 7, no. 10, Apr. 2019, pp. 9680-9689. https://doi.org/10.1021/acssuschemeng.9b01405.
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