Anionic Pd(0) and Pd(II) Intermediates in Palladium-Catalyzed Heck and Cross-Coupling Reactions
1
Département de Chimie, Ecole Normale Supérieure, CNRS UMR 8640, 24 Rue Lhomond, F-75231 Paris Cedex 5, France
|
Publication type: Journal Article
Publication date: 2000-03-11
scimago Q1
wos Q1
SJR: 5.433
CiteScore: 30.7
Impact factor: 17.7
ISSN: 00014842, 15204898
PubMed ID:
10813876
General Chemistry
General Medicine
Abstract
The anions of PdCl(2)L(2) and Pd(OAc)(2), precursors of palladium(0) used in cross-coupling and Heck reactions, play a crucial role in these reactions. Tricoordinated anionic complexes Pd(0)L(2)Cl(-) and Pd(0)L(2)(OAc)(-) are the effective catalysts instead of the usually postulated Pd(0)L(2) complex. The anion ligated to the palladium(0) affects the kinetics of the oxidative addition to ArI as well as the structure and reactivity of the arylpalladium(II) complexes produced in this reaction. Thus, pentacoordinated anionic complexes are formed, ArPdI(Cl)L(2)(-) or ArPdI(OAc)L(2)(-), the precursor of neutral trans-ArPd(OAc)L(2), instead of the usually postulated trans-ArPdIL(2) complex (L = PPh(3)).
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Amatore C., Jutand A. Anionic Pd(0) and Pd(II) Intermediates in Palladium-Catalyzed Heck and Cross-Coupling Reactions // Accounts of Chemical Research. 2000. Vol. 33. No. 5. pp. 314-321.
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Amatore C., Jutand A. Anionic Pd(0) and Pd(II) Intermediates in Palladium-Catalyzed Heck and Cross-Coupling Reactions // Accounts of Chemical Research. 2000. Vol. 33. No. 5. pp. 314-321.
Cite this
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TY - JOUR
DO - 10.1021/ar980063a
UR - https://doi.org/10.1021/ar980063a
TI - Anionic Pd(0) and Pd(II) Intermediates in Palladium-Catalyzed Heck and Cross-Coupling Reactions
T2 - Accounts of Chemical Research
AU - Amatore, Christian
AU - Jutand, Anny
PY - 2000
DA - 2000/03/11
PB - American Chemical Society (ACS)
SP - 314-321
IS - 5
VL - 33
PMID - 10813876
SN - 0001-4842
SN - 1520-4898
ER -
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BibTex (up to 50 authors)
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@article{2000_Amatore,
author = {Christian Amatore and Anny Jutand},
title = {Anionic Pd(0) and Pd(II) Intermediates in Palladium-Catalyzed Heck and Cross-Coupling Reactions},
journal = {Accounts of Chemical Research},
year = {2000},
volume = {33},
publisher = {American Chemical Society (ACS)},
month = {mar},
url = {https://doi.org/10.1021/ar980063a},
number = {5},
pages = {314--321},
doi = {10.1021/ar980063a}
}
Cite this
MLA
Copy
Amatore, Christian, and Anny Jutand. “Anionic Pd(0) and Pd(II) Intermediates in Palladium-Catalyzed Heck and Cross-Coupling Reactions.” Accounts of Chemical Research, vol. 33, no. 5, Mar. 2000, pp. 314-321. https://doi.org/10.1021/ar980063a.