Chiral Templating Activity of Tris(bipyridine)ruthenium(II) Cation in the Design of Three-Dimensional (3D) Optically Active Oxalate-Bridged {[Ru(bpy)3][Cu2xNi2(1-x)(C2O4)3]}n (0 ≤ x ≤ 1; bpy = 2,2‘-bipyridine): Structural, Optical, and Magnetic Studies
Тип публикации: Journal Article
Дата публикации: 2004-02-13
scimago Q1
wos Q1
БС1
SJR: 2.065
CiteScore: 12
Impact factor: 7
ISSN: 08974756, 15205002
Materials Chemistry
General Chemistry
General Chemical Engineering
Краткое описание
Three-dimensional oxalate-based {[Ru(bpy)3][Cu2xNi2(1-x)(ox)3]}n (0≤ x ≤ 1, ox = C2O42-, bpy = 2,2‘bipyridine) were synthesized. The structure was determined for x = 1 by X-ray diffraction on single crystal. The compound crystallizes in the cubic space group P4132. It shows a three-dimensional 10-gon 3-connected (10,3) anionic network where copper(II) has an unusual tris(bischelated) environment. X-ray powder diffraction patterns and their Rietveld refinement show that all the compounds along the series are isostructural and single-phased. According to X-ray absorption spectroscopy, copper(II) and nickel(II) have an octahedral environment, respectively elongated and trigonally distorted. As shown by natural circular dichroism, the optically active forms of {[Ru(bpy)3][CuxNi2(1-x)(ox)3]}n are obtained starting from resolved Δ- or Λ-[Ru(bpy)3]2+. The Curie−Weiss temperatures range between −55 (x = 1) and −150 K (x = 0). The antiferromagnetic exchange interaction thus decreases when the copper contents incre...
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Pointillart F. et al. Chiral Templating Activity of Tris(bipyridine)ruthenium(II) Cation in the Design of Three-Dimensional (3D) Optically Active Oxalate-Bridged {[Ru(bpy)3][Cu2xNi2(1-x)(C2O4)3]}n (0 ≤ x ≤ 1; bpy = 2,2‘-bipyridine): Structural, Optical, and Magnetic Studies // Chemistry of Materials. 2004. Vol. 16. No. 5. pp. 832-841.
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Pointillart F., Train C., Gruselle M., Villain F., Schmalle H. W., Talbot D., Gredin P., Decurtins S., Verdaguer M. Chiral Templating Activity of Tris(bipyridine)ruthenium(II) Cation in the Design of Three-Dimensional (3D) Optically Active Oxalate-Bridged {[Ru(bpy)3][Cu2xNi2(1-x)(C2O4)3]}n (0 ≤ x ≤ 1; bpy = 2,2‘-bipyridine): Structural, Optical, and Magnetic Studies // Chemistry of Materials. 2004. Vol. 16. No. 5. pp. 832-841.
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TY - JOUR
DO - 10.1021/cm020330d
UR - https://doi.org/10.1021/cm020330d
TI - Chiral Templating Activity of Tris(bipyridine)ruthenium(II) Cation in the Design of Three-Dimensional (3D) Optically Active Oxalate-Bridged {[Ru(bpy)3][Cu2xNi2(1-x)(C2O4)3]}n (0 ≤ x ≤ 1; bpy = 2,2‘-bipyridine): Structural, Optical, and Magnetic Studies
T2 - Chemistry of Materials
AU - Pointillart, Fabrice
AU - Train, Cyrille
AU - Gruselle, Michel
AU - Villain, Francoise
AU - Schmalle, Helmut W.
AU - Talbot, Delphine
AU - Gredin, Patrick
AU - Decurtins, Silvio
AU - Verdaguer, Michel
PY - 2004
DA - 2004/02/13
PB - American Chemical Society (ACS)
SP - 832-841
IS - 5
VL - 16
SN - 0897-4756
SN - 1520-5002
ER -
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@article{2004_Pointillart,
author = {Fabrice Pointillart and Cyrille Train and Michel Gruselle and Francoise Villain and Helmut W. Schmalle and Delphine Talbot and Patrick Gredin and Silvio Decurtins and Michel Verdaguer},
title = {Chiral Templating Activity of Tris(bipyridine)ruthenium(II) Cation in the Design of Three-Dimensional (3D) Optically Active Oxalate-Bridged {[Ru(bpy)3][Cu2xNi2(1-x)(C2O4)3]}n (0 ≤ x ≤ 1; bpy = 2,2‘-bipyridine): Structural, Optical, and Magnetic Studies},
journal = {Chemistry of Materials},
year = {2004},
volume = {16},
publisher = {American Chemical Society (ACS)},
month = {feb},
url = {https://doi.org/10.1021/cm020330d},
number = {5},
pages = {832--841},
doi = {10.1021/cm020330d}
}
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Pointillart, Fabrice, et al. “Chiral Templating Activity of Tris(bipyridine)ruthenium(II) Cation in the Design of Three-Dimensional (3D) Optically Active Oxalate-Bridged {[Ru(bpy)3][Cu2xNi2(1-x)(C2O4)3]}n (0 ≤ x ≤ 1; bpy = 2,2‘-bipyridine): Structural, Optical, and Magnetic Studies.” Chemistry of Materials, vol. 16, no. 5, Feb. 2004, pp. 832-841. https://doi.org/10.1021/cm020330d.