Crystal structure of a lightweight borohydride from submicrometer crystallites by precession electron diffraction
Publication type: Journal Article
Publication date: 2012-08-22
scimago Q1
wos Q1
SJR: 2.065
CiteScore: 12.0
Impact factor: 7.0
ISSN: 08974756, 15205002
Materials Chemistry
General Chemistry
General Chemical Engineering
Abstract
We demonstrate that precession electron diffraction at low-dose conditions can be successfully applied for structure analysis of extremely electron-beam-sensitive materials. Using LiBH4 as a test material, complete structural information, including the location of the H atoms, was obtained from submicrometer-sized crystallites. This demonstrates for the first time that, where conventional transmission electron microscopy techniques fail, quantitative precession electron diffraction can provide structural information from submicrometer particles of such extremely electron-beam-sensitive materials as complex lightweight hydrides. We expect the precession electron diffraction technique to be a useful tool for nanoscale investigations of thermally unstable lightweight hydrogen-storage materials.
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Metrics
18
Total citations:
18
Citations from 2024:
0
The most citing journal
Citations in journal:
5
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MLA
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GOST
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Hadermann J. et al. Crystal structure of a lightweight borohydride from submicrometer crystallites by precession electron diffraction // Chemistry of Materials. 2012. Vol. 24. No. 17. pp. 3401-3405.
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Hadermann J., Abakumov A. M., Van Rompaey S., Perkisas T., Filinchuk Y., Van Tendeloo G. Crystal structure of a lightweight borohydride from submicrometer crystallites by precession electron diffraction // Chemistry of Materials. 2012. Vol. 24. No. 17. pp. 3401-3405.
Cite this
RIS
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TY - JOUR
DO - 10.1021/cm301548k
UR - https://doi.org/10.1021/cm301548k
TI - Crystal structure of a lightweight borohydride from submicrometer crystallites by precession electron diffraction
T2 - Chemistry of Materials
AU - Hadermann, Joke
AU - Abakumov, Artem M.
AU - Van Rompaey, Senne
AU - Perkisas, Tyché
AU - Filinchuk, Yaroslav
AU - Van Tendeloo, Gustaaf
PY - 2012
DA - 2012/08/22
PB - American Chemical Society (ACS)
SP - 3401-3405
IS - 17
VL - 24
SN - 0897-4756
SN - 1520-5002
ER -
Cite this
BibTex (up to 50 authors)
Copy
@article{2012_Hadermann,
author = {Joke Hadermann and Artem M. Abakumov and Senne Van Rompaey and Tyché Perkisas and Yaroslav Filinchuk and Gustaaf Van Tendeloo},
title = {Crystal structure of a lightweight borohydride from submicrometer crystallites by precession electron diffraction},
journal = {Chemistry of Materials},
year = {2012},
volume = {24},
publisher = {American Chemical Society (ACS)},
month = {aug},
url = {https://doi.org/10.1021/cm301548k},
number = {17},
pages = {3401--3405},
doi = {10.1021/cm301548k}
}
Cite this
MLA
Copy
Hadermann, Joke, et al. “Crystal structure of a lightweight borohydride from submicrometer crystallites by precession electron diffraction.” Chemistry of Materials, vol. 24, no. 17, Aug. 2012, pp. 3401-3405. https://doi.org/10.1021/cm301548k.
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