Nickel-Catalyzed Amination of Aryl Chlorides and Sulfamates in 2-Methyl-THF
Тип публикации: Journal Article
Дата публикации: 2014-08-27
SCImago Q1
Tоп 10% SCImago
WOS Q1
БС1
SJR: 3.541
CiteScore: 19.5
Impact factor: 13.1
ISSN: 21555435
PubMed ID:
25243095
General Chemistry
Catalysis
Краткое описание
The nickel-catalyzed amination of aryl O-sulfamates and chlorides using the green solvent 2-methyl-THF is reported. This methodology employs the commercially available and air-stable precatalyst NiCl2(DME), is broad in scope, and provides access to aryl amines in synthetically useful yields. The utility of this methodology is underscored by examples of gram-scale couplings conducted with catalyst loadings as low as 1 mol % nickel. Moreover, the nickel-catalyzed amination described is tolerant of heterocycles and should prove useful in the synthesis of pharmaceutical candidates and other heteroatom-containing compounds.
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ГОСТ
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Fine Nathel N. F. et al. Nickel-Catalyzed Amination of Aryl Chlorides and Sulfamates in 2-Methyl-THF // ACS Catalysis. 2014. Vol. 4. No. 9. pp. 3289-3293.
ГОСТ со всеми авторами (до 50)
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Fine Nathel N. F., Kim J., Hie L., Jiang X., Garg N. K. Nickel-Catalyzed Amination of Aryl Chlorides and Sulfamates in 2-Methyl-THF // ACS Catalysis. 2014. Vol. 4. No. 9. pp. 3289-3293.
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RIS
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TY - JOUR
DO - 10.1021/cs501045v
UR - https://doi.org/10.1021/cs501045v
TI - Nickel-Catalyzed Amination of Aryl Chlorides and Sulfamates in 2-Methyl-THF
T2 - ACS Catalysis
AU - Fine Nathel, Noah F
AU - Kim, Junyong
AU - Hie, Liana
AU - Jiang, Xingyu
AU - Garg, Neil K
PY - 2014
DA - 2014/08/27
PB - American Chemical Society (ACS)
SP - 3289-3293
IS - 9
VL - 4
PMID - 25243095
SN - 2155-5435
ER -
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BibTex (до 50 авторов)
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@article{2014_Fine Nathel,
author = {Noah F Fine Nathel and Junyong Kim and Liana Hie and Xingyu Jiang and Neil K Garg},
title = {Nickel-Catalyzed Amination of Aryl Chlorides and Sulfamates in 2-Methyl-THF},
journal = {ACS Catalysis},
year = {2014},
volume = {4},
publisher = {American Chemical Society (ACS)},
month = {aug},
url = {https://doi.org/10.1021/cs501045v},
number = {9},
pages = {3289--3293},
doi = {10.1021/cs501045v}
}
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MLA
Скопировать
Fine Nathel, Noah F., et al. “Nickel-Catalyzed Amination of Aryl Chlorides and Sulfamates in 2-Methyl-THF.” ACS Catalysis, vol. 4, no. 9, Aug. 2014, pp. 3289-3293. https://doi.org/10.1021/cs501045v.
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