"Anti-Crown" Chemistry: Synthesis of (9)Mercuracarborand-3 and the Crystal Structure of Its Acetonitrile Complexes
Тип публикации: Journal Article
Дата публикации: 1993-01-01
SCImago Q1
Tоп 10% SCImago
WOS Q1
БС1
SJR: 5.491
CiteScore: 22
Impact factor: 16.6
ISSN: 00027863, 15205126
General Chemistry
Catalysis
Biochemistry
Colloid and Surface Chemistry
Краткое описание
The reaction of mercuric acetate with closo-1 ,2-Li2-1 ,2-C2BloHlo yielded (9)mercuracarborand-3, (C2BloHloHg), (l), in 60% yield. Compound 1 was characterized by multinuclear NMR spectroscopy and its chloride ion complex, l.CI-, by negative ion FAB mass spectroscopy. The structure of 1 was determined by X-ray crystallography. 1 crystallized from acetonitrile in the monoclinic space group P21/c with a = 13.358 (2), b = 26.846 (4), and c = 20.375 A, 0 = 109.694 (S)", V = 7909 AS, and 2 = 4. Data were collected on a Picker FACS-1 diffractometer, using Mo Ka radiation, to a maximum 20 = 45", giving 10 348 unique reflections, and the structure was solved by heavy atom methods. The final discrepancy index was R = 0.044, R, = 0.049 for 5193 independent reflections with I > 34). The chloride ion complex of 1, IClLi, was formed upon treatment of 1 with LiCI. The complexation behavior of 1 in acetone was studied by 199Hg NMR spectroscopy.
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Yang X. et al. "Anti-Crown" Chemistry: Synthesis of (9)Mercuracarborand-3 and the Crystal Structure of Its Acetonitrile Complexes // Journal of the American Chemical Society. 1993. Vol. 115. No. 1. pp. 193-195.
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Yang X., Zheng Z., Knobler C. B., Hawthorne M. F. "Anti-Crown" Chemistry: Synthesis of (9)Mercuracarborand-3 and the Crystal Structure of Its Acetonitrile Complexes // Journal of the American Chemical Society. 1993. Vol. 115. No. 1. pp. 193-195.
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TY - JOUR
DO - 10.1021/ja00054a026
UR - https://doi.org/10.1021/ja00054a026
TI - "Anti-Crown" Chemistry: Synthesis of (9)Mercuracarborand-3 and the Crystal Structure of Its Acetonitrile Complexes
T2 - Journal of the American Chemical Society
AU - Yang, Xiaoguang
AU - Zheng, Zhiping
AU - Knobler, Carolyn B.
AU - Hawthorne, M Frederick
PY - 1993
DA - 1993/01/01
PB - American Chemical Society (ACS)
SP - 193-195
IS - 1
VL - 115
SN - 0002-7863
SN - 1520-5126
ER -
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BibTex (до 50 авторов)
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@article{1993_Yang,
author = {Xiaoguang Yang and Zhiping Zheng and Carolyn B. Knobler and M Frederick Hawthorne},
title = {"Anti-Crown" Chemistry: Synthesis of (9)Mercuracarborand-3 and the Crystal Structure of Its Acetonitrile Complexes},
journal = {Journal of the American Chemical Society},
year = {1993},
volume = {115},
publisher = {American Chemical Society (ACS)},
month = {jan},
url = {https://doi.org/10.1021/ja00054a026},
number = {1},
pages = {193--195},
doi = {10.1021/ja00054a026}
}
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MLA
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Yang, Xiaoguang, et al. “"Anti-Crown" Chemistry: Synthesis of (9)Mercuracarborand-3 and the Crystal Structure of Its Acetonitrile Complexes.” Journal of the American Chemical Society, vol. 115, no. 1, Jan. 1993, pp. 193-195. https://doi.org/10.1021/ja00054a026.
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