Journal of the American Chemical Society, volume 133, issue 46, pages 18610-18613
Synthesis of poly(indene carbonate) from indene oxide and carbon dioxide--a polycarbonate with a rigid backbone.
Publication type: Journal Article
Publication date: 2011-11-01
Q1
Q1
SJR: 5.489
CiteScore: 24.4
Impact factor: 14.4
ISSN: 00027863, 15205126
General Chemistry
Catalysis
Biochemistry
Colloid and Surface Chemistry
Abstract
The catalytic coupling of carbon dioxide with indene oxide utilizing (salen)Co(III)-2,4-dinitrophenoxide in the presence of an onium salt is presented. X-ray structural data for indene oxide monomer as well as cis-indene carbonate display near planarity of the fused cyclopentene and benzene rings. Low temperature (0 °C) is required to selectively afford copolymer vs cyclic carbonate from the coupling reactions of CO(2) and indene oxide. The produced poly(indene carbonate) samples have molecular weights of up to 7100 Da, with corresponding glass transition temperatures of up to 134 °C, the highest yet reported for polycarbonates produced from CO(2)/epoxides coupling. Poly(indene carbonate) is thermally stable up to 249 °C. The polymerizations are well controlled, with PDI values ≤1.3.
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Darensbourg D. J., Wilson S. J. Synthesis of poly(indene carbonate) from indene oxide and carbon dioxide--a polycarbonate with a rigid backbone. // Journal of the American Chemical Society. 2011. Vol. 133. No. 46. pp. 18610-18613.
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Darensbourg D. J., Wilson S. J. Synthesis of poly(indene carbonate) from indene oxide and carbon dioxide--a polycarbonate with a rigid backbone. // Journal of the American Chemical Society. 2011. Vol. 133. No. 46. pp. 18610-18613.
Cite this
RIS
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TY - JOUR
DO - 10.1021/ja208711c
UR - https://doi.org/10.1021/ja208711c
TI - Synthesis of poly(indene carbonate) from indene oxide and carbon dioxide--a polycarbonate with a rigid backbone.
T2 - Journal of the American Chemical Society
AU - Darensbourg, Donald J.
AU - Wilson, Stephanie J.
PY - 2011
DA - 2011/11/01
PB - American Chemical Society (ACS)
SP - 18610-18613
IS - 46
VL - 133
SN - 0002-7863
SN - 1520-5126
ER -
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BibTex (up to 50 authors)
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@article{2011_Darensbourg,
author = {Donald J. Darensbourg and Stephanie J. Wilson},
title = {Synthesis of poly(indene carbonate) from indene oxide and carbon dioxide--a polycarbonate with a rigid backbone.},
journal = {Journal of the American Chemical Society},
year = {2011},
volume = {133},
publisher = {American Chemical Society (ACS)},
month = {nov},
url = {https://doi.org/10.1021/ja208711c},
number = {46},
pages = {18610--18613},
doi = {10.1021/ja208711c}
}
Cite this
MLA
Copy
Darensbourg, Donald J., and Stephanie J. Wilson. “Synthesis of poly(indene carbonate) from indene oxide and carbon dioxide--a polycarbonate with a rigid backbone..” Journal of the American Chemical Society, vol. 133, no. 46, Nov. 2011, pp. 18610-18613. https://doi.org/10.1021/ja208711c.