Journal of the American Chemical Society, volume 130, issue 45, pages 15203-15209

Simple Cubic Super Crystals Containing PbTe Nanocubes and Their Core−Shell Building Blocks

Jun Zhang ¹

Amar Kumbhar ¹

J. He ¹

Narayan Das ¹

Kaikun Yang ¹

Jian-Qing Wang ¹

Howard Wang ¹

Kevin L. Stokes ¹

Jiye Fang ¹

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Department of Chemistry, State University of New York at Binghamton, Binghamton, New York 13902, Electron Microscope Facility, Clemson University, Anderson, South Carolina 29625, Coordinated Instrumentation Facility, Tulane University, New Orleans, Louisiana 70118, Department of Mechanical Engineering, State University of New York at Binghamton, Binghamton, New York 13902, Department of Physics, State University of New York at Binghamton, Binghamton, New York 13902, and Department of Physics, University...

Publication type: Journal Article

Publication date: 2008-10-21

American Chemical Society (ACS)

Journal: Journal of the American Chemical Society

scimago Q1

SJR: 5.489

CiteScore: 24.4

Impact factor: 14.4

ISSN: 00027863, 15205126

DOI: 10.1021/ja806120w

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PubMed ID: 18937469

General Chemistry

Catalysis

Biochemistry

Colloid and Surface Chemistry

Abstract

We report a preparation of high-quality cubic PbTe nanocrystals and their assembly into both square-array, two-dimensional patterns and three-dimensional simple cubic super crystals. The influence of oleylamine in the nanocrystal synthesis and core-shell formation through an anion-exchange mechanism was also studied. The simple cubic super crystals together with two-dimensional assembly patterns containing PbTe nanocubes and their core-shell building blocks were examined using TEM, SEM, AFM, XRD, SAXS, and FTIR. Such super crystals consisting of cubic structural building blocks may allow engineering of more complex materials from which novel properties may emerge.

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