Nickel-Catalyzed Carbonylative Negishi Cross-Coupling of Unactivated Secondary Alkyl Electrophiles with 1 atm CO Gas
Тип публикации: Journal Article
Дата публикации: 2024-03-14
SCImago Q1
Tоп 10% SCImago
WOS Q1
БС1
SJR: 5.491
CiteScore: 22.5
Impact factor: 15.6
ISSN: 00027863, 15205126
PubMed ID:
38483538
General Chemistry
Catalysis
Biochemistry
Colloid and Surface Chemistry
Краткое описание
We describe a nickel-catalyzed carbonylative cross-coupling of unactivated secondary alkyl electrophiles with the organozinc reagent at atmospheric CO gas, thus allowing the expedient construction of unsymmetric dialkyl ketones with broad functional group tolerance. The leverage of a newly developed NN2-pincer type ligand enables the chemoselective three-component carbonylation by overcoming the competing Negishi coupling, the undesired β-hydride elimination, and dehalogenation of alkyl iodides side pathways. Both alkyl iodides and alkyl tosylates are compatible in the single electron transfer involved mechanism.
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Zhang Y. et al. Nickel-Catalyzed Carbonylative Negishi Cross-Coupling of Unactivated Secondary Alkyl Electrophiles with 1 atm CO Gas // Journal of the American Chemical Society. 2024. Vol. 146. No. 12. pp. 7971-7978.
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Zhang Y., Cao Q., Xi Y., Wu X., Qu J., Chen Y. Nickel-Catalyzed Carbonylative Negishi Cross-Coupling of Unactivated Secondary Alkyl Electrophiles with 1 atm CO Gas // Journal of the American Chemical Society. 2024. Vol. 146. No. 12. pp. 7971-7978.
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TY - JOUR
DO - 10.1021/jacs.4c02023
UR - https://pubs.acs.org/doi/10.1021/jacs.4c02023
TI - Nickel-Catalyzed Carbonylative Negishi Cross-Coupling of Unactivated Secondary Alkyl Electrophiles with 1 atm CO Gas
T2 - Journal of the American Chemical Society
AU - Zhang, Yetong
AU - Cao, Qihang
AU - Xi, Yang
AU - Wu, Xianqing
AU - Qu, Jingping
AU - Chen, Yifeng
PY - 2024
DA - 2024/03/14
PB - American Chemical Society (ACS)
SP - 7971-7978
IS - 12
VL - 146
PMID - 38483538
SN - 0002-7863
SN - 1520-5126
ER -
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BibTex (до 50 авторов)
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@article{2024_Zhang,
author = {Yetong Zhang and Qihang Cao and Yang Xi and Xianqing Wu and Jingping Qu and Yifeng Chen},
title = {Nickel-Catalyzed Carbonylative Negishi Cross-Coupling of Unactivated Secondary Alkyl Electrophiles with 1 atm CO Gas},
journal = {Journal of the American Chemical Society},
year = {2024},
volume = {146},
publisher = {American Chemical Society (ACS)},
month = {mar},
url = {https://pubs.acs.org/doi/10.1021/jacs.4c02023},
number = {12},
pages = {7971--7978},
doi = {10.1021/jacs.4c02023}
}
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MLA
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Zhang, Yetong, et al. “Nickel-Catalyzed Carbonylative Negishi Cross-Coupling of Unactivated Secondary Alkyl Electrophiles with 1 atm CO Gas.” Journal of the American Chemical Society, vol. 146, no. 12, Mar. 2024, pp. 7971-7978. https://pubs.acs.org/doi/10.1021/jacs.4c02023.
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