Cyclohexyl rings in spatial proximity: stereochemistry of tricyclohexylmethane
Тип публикации: Journal Article
Дата публикации: 1993-12-01
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wos Q1
БС1
SJR: 0.737
CiteScore: 6.1
Impact factor: 3.6
ISSN: 00223263, 15206904
Organic Chemistry
Краткое описание
The static and dynamic stereochemistry of tricyclohexylmethane (2) is analyzed. The 13 C and 1 H NMR of (2) were assigned by means of the 2D NMR techniques INADEQUATE and DQF COSY. Molecular mechanics calculations were performed in order to estimate the influence of the torsional angles of the cyclohexyl rings and their mode of attachment (equatorial or axial) on the relative energy of the conformations. MM3 calculations of (2) indicate that in the lowest energy conformation the cyclohexyl rings are attached to the central carbon via their equatorial positions and are oriented in a chiral gauche,gauche,anti (g,g,a) arrangement. The compound crystallizes in two crystalline forms
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Columbus I., Biali S. E. Cyclohexyl rings in spatial proximity: stereochemistry of tricyclohexylmethane // Journal of Organic Chemistry. 1993. Vol. 58. No. 25. pp. 7029-7035.
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Columbus I., Biali S. E. Cyclohexyl rings in spatial proximity: stereochemistry of tricyclohexylmethane // Journal of Organic Chemistry. 1993. Vol. 58. No. 25. pp. 7029-7035.
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TY - JOUR
DO - 10.1021/jo00077a021
UR - https://doi.org/10.1021/jo00077a021
TI - Cyclohexyl rings in spatial proximity: stereochemistry of tricyclohexylmethane
T2 - Journal of Organic Chemistry
AU - Columbus, Ishay
AU - Biali, Silvio E
PY - 1993
DA - 1993/12/01
PB - American Chemical Society (ACS)
SP - 7029-7035
IS - 25
VL - 58
SN - 0022-3263
SN - 1520-6904
ER -
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@article{1993_Columbus,
author = {Ishay Columbus and Silvio E Biali},
title = {Cyclohexyl rings in spatial proximity: stereochemistry of tricyclohexylmethane},
journal = {Journal of Organic Chemistry},
year = {1993},
volume = {58},
publisher = {American Chemical Society (ACS)},
month = {dec},
url = {https://doi.org/10.1021/jo00077a021},
number = {25},
pages = {7029--7035},
doi = {10.1021/jo00077a021}
}
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MLA
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Columbus, Ishay, and Silvio E Biali. “Cyclohexyl rings in spatial proximity: stereochemistry of tricyclohexylmethane.” Journal of Organic Chemistry, vol. 58, no. 25, Dec. 1993, pp. 7029-7035. https://doi.org/10.1021/jo00077a021.