Journal of Organic Chemistry

, volume 78 , issue 8 , pages 3767-3773

Preparation and X-ray structural study of 1-arylbenziodoxolones.

Mekhman S. Yusubov ¹

Roza Y Yusubova ¹

Victor V. Nemykin ²

Viktor V. Zhdankin ²

Hide authors affiliations Show authors affiliations: 2 affiliations

The Siberian State Medical University and The Tomsk Polytechnic University, 634050 Tomsk, Russia

National Research Tomsk Polytechnic University

Siberian State Medical University

Department of Chemistry and Biochemistry, University of Minnesota Duluth, Duluth, Minnesota, 55812, United States |

Publication type: Journal Article

Publication date: 2013-03-21

American Chemical Society (ACS)

Journal of Organic Chemistry

scimago Q2

wos Q1

SJR: 0.737

CiteScore: 6.1

Impact factor: 3.6

ISSN: 00223263, 15206904

DOI: 10.1021/jo400212u

Copy DOI

PubMed ID: 23480389

Organic Chemistry

Abstract

Various 1-arylbenziodoxolones can be conveniently prepared from 2-iodobenzoic acid and arenes by a one-pot procedure using Oxone (2KHSO5·KHSO4·K2SO4) as an inexpensive and environmentally safe oxidant. This procedure is also applicable for the synthesis of the 7-methylbenziodoxolone ring system using 2-iodo-3-methylbenzoic acid as starting compound. Structures of four 1-arylbenziodoxolone derivatives were established by single-crystal X-ray diffraction analysis. An enhanced reactivity of 1-aryl-7-methylbenziodoxolones toward nucleophiles compared to unsubstituted 1-arylbenziodoxolones has been found.

Found

10 citations

Postnikov Pavel

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National Research Tomsk Polytechnic University

N.N. Vorozhtsov Novosibirsk Institute of Organic Chemistry of the Siberian Branch of the Russian Academy of Sciences

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North Caucasus Federal University

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GOST |

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S. Yusubov M. et al. Preparation and X-ray structural study of 1-arylbenziodoxolones. // Journal of Organic Chemistry. 2013. Vol. 78. No. 8. pp. 3767-3773.

GOST all authors (up to 50) Copy

S. Yusubov M., Yusubova R. Y., Nemykin V. V., Zhdankin V. V. Preparation and X-ray structural study of 1-arylbenziodoxolones. // Journal of Organic Chemistry. 2013. Vol. 78. No. 8. pp. 3767-3773.

RIS |

Cite this

RIS Copy

TY - JOUR

DO - 10.1021/jo400212u

UR - https://doi.org/10.1021/jo400212u

TI - Preparation and X-ray structural study of 1-arylbenziodoxolones.

T2 - Journal of Organic Chemistry

AU - S. Yusubov, Mekhman

AU - Yusubova, Roza Y

AU - Nemykin, Victor V.

AU - Zhdankin, Viktor V.

PY - 2013

DA - 2013/03/21

PB - American Chemical Society (ACS)

SP - 3767-3773

IS - 8

VL - 78

PMID - 23480389

SN - 0022-3263

SN - 1520-6904

ER -

BibTex |

Cite this

BibTex (up to 50 authors) Copy

@article{2013_S. Yusubov,

author = {Mekhman S. Yusubov and Roza Y Yusubova and Victor V. Nemykin and Viktor V. Zhdankin},

title = {Preparation and X-ray structural study of 1-arylbenziodoxolones.},

journal = {Journal of Organic Chemistry},

year = {2013},

volume = {78},

publisher = {American Chemical Society (ACS)},

month = {mar},

url = {https://doi.org/10.1021/jo400212u},

number = {8},

pages = {3767--3773},

doi = {10.1021/jo400212u}

}

MLA

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MLA Copy

S. Yusubov, Mekhman, et al. “Preparation and X-ray structural study of 1-arylbenziodoxolones..” Journal of Organic Chemistry, vol. 78, no. 8, Mar. 2013, pp. 3767-3773. https://doi.org/10.1021/jo400212u.

Publisher

American Chemical Society (ACS)

Journal

Journal of Organic Chemistry

scimago Q2

wos Q1

SJR

0.737

CiteScore

6.1

Impact factor

3.6

ISSN

00223263 (Print)

15206904 (Electronic)