Distinction between Light and Heavy Lanthanide(III) Ions Based on the 1H NMR Spectra of Heteroleptic Triple-Decker Phthalocyaninato Sandwich Complexes
Тип публикации: Journal Article
Дата публикации: 2001-07-21
SCImago Q2
WOS Q2
БС2
SJR: 0.62
CiteScore: 4.8
Impact factor: 2.8
ISSN: 10895639, 15205215
Physical and Theoretical Chemistry
Краткое описание
The 1H NMR spectra of two series of heteroleptic triple-decker phthalocyaninato sandwich complexes of the rare earth(III) ions have been recorded. The ligands comprise unsubstituted phthalocyanine (Pc) and 2,3,9,10,16,17,23,24-octakis(1‘-octyloxy)phthalocyanine (Pc*), and the complexes are of the form PcMPc*MPc (series 1) and PcMPc*MPc* (series 2), where M = Pr − Tm (except Pm, Gd). In some cases, the homoleptic complexes Pc*MPc*MPc* (series 3) were also available. The chemical shifts of five proton positions in series 1, and 10 positions in series 2 were compared with the shifts for the analogous complexes of the diamagnetic yttrium(III) ion. The experimental lanthanide-induced shifts (LIS) were separated into the contact and dipolar contributions using the crystal-field dependent methods of Reilley and co-workers. This work represents the first analysis of LIS in triple-decker phthalocyaninato lanthanide complexes. The results showed a dominance of dipolar contributions but also revealed that contact in...
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Arnold D. P., Jiang J. Distinction between Light and Heavy Lanthanide(III) Ions Based on the 1H NMR Spectra of Heteroleptic Triple-Decker Phthalocyaninato Sandwich Complexes // Journal of Physical Chemistry A. 2001. Vol. 105. No. 32. pp. 7525-7533.
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Arnold D. P., Jiang J. Distinction between Light and Heavy Lanthanide(III) Ions Based on the 1H NMR Spectra of Heteroleptic Triple-Decker Phthalocyaninato Sandwich Complexes // Journal of Physical Chemistry A. 2001. Vol. 105. No. 32. pp. 7525-7533.
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TY - JOUR
DO - 10.1021/jp0105847
UR - https://doi.org/10.1021/jp0105847
TI - Distinction between Light and Heavy Lanthanide(III) Ions Based on the 1H NMR Spectra of Heteroleptic Triple-Decker Phthalocyaninato Sandwich Complexes
T2 - Journal of Physical Chemistry A
AU - Arnold, Dennis P.
AU - Jiang, Jianzhuang
PY - 2001
DA - 2001/07/21
PB - American Chemical Society (ACS)
SP - 7525-7533
IS - 32
VL - 105
SN - 1089-5639
SN - 1520-5215
ER -
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@article{2001_Arnold,
author = {Dennis P. Arnold and Jianzhuang Jiang},
title = {Distinction between Light and Heavy Lanthanide(III) Ions Based on the 1H NMR Spectra of Heteroleptic Triple-Decker Phthalocyaninato Sandwich Complexes},
journal = {Journal of Physical Chemistry A},
year = {2001},
volume = {105},
publisher = {American Chemical Society (ACS)},
month = {jul},
url = {https://doi.org/10.1021/jp0105847},
number = {32},
pages = {7525--7533},
doi = {10.1021/jp0105847}
}
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Arnold, Dennis P., and Jianzhuang Jiang. “Distinction between Light and Heavy Lanthanide(III) Ions Based on the 1H NMR Spectra of Heteroleptic Triple-Decker Phthalocyaninato Sandwich Complexes.” Journal of Physical Chemistry A, vol. 105, no. 32, Jul. 2001, pp. 7525-7533. https://doi.org/10.1021/jp0105847.
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