NMR Relaxation Study of the Protonated Form of 1,8-Bis(dimethylamino)naphthalene in Isotropic Solution: Anisotropic Motion outside of Extreme Narrowing and Ultrafast Proton Transfer
Тип публикации: Journal Article
Дата публикации: 2004-12-09
scimago Q2
wos Q2
БС2
SJR: 0.634
CiteScore: 4.8
Impact factor: 2.8
ISSN: 10895639, 15205215
PubMed ID:
16839089
Physical and Theoretical Chemistry
Краткое описание
The protonated form of 1,8-bis(dimethylamino)naphthalene (DMANH(+)) consists of a rigid, aromatic framework, substituted by two amino groups that are connected by a strong, symmetric (on the NMR time-scale) hydrogen bond bridge. The reorientational motion of the molecule in dimethylformamide-d7 solution was characterized by T(1) and NOE measurements for aromatic (13)C nuclei. Treating the reorientation of DMANH(+) as anisotropic rotational diffusion of a rigid body, the diffusion tensor was determined with good accuracy. Measurements and interpretation of (15)N T(1) and NOE indicate that the proton transfer between potential minima in the hydrogen bond bridge is faster than the molecular reorientation.
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Bernatowicz P., Kowalewski J., Sandström D. NMR Relaxation Study of the Protonated Form of 1,8-Bis(dimethylamino)naphthalene in Isotropic Solution: Anisotropic Motion outside of Extreme Narrowing and Ultrafast Proton Transfer // Journal of Physical Chemistry A. 2004. Vol. 109. No. 1. pp. 57-63.
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Bernatowicz P., Kowalewski J., Sandström D. NMR Relaxation Study of the Protonated Form of 1,8-Bis(dimethylamino)naphthalene in Isotropic Solution: Anisotropic Motion outside of Extreme Narrowing and Ultrafast Proton Transfer // Journal of Physical Chemistry A. 2004. Vol. 109. No. 1. pp. 57-63.
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TY - JOUR
DO - 10.1021/jp045454n
UR - https://doi.org/10.1021/jp045454n
TI - NMR Relaxation Study of the Protonated Form of 1,8-Bis(dimethylamino)naphthalene in Isotropic Solution: Anisotropic Motion outside of Extreme Narrowing and Ultrafast Proton Transfer
T2 - Journal of Physical Chemistry A
AU - Bernatowicz, Piotr
AU - Kowalewski, Jozef
AU - Sandström, Dick
PY - 2004
DA - 2004/12/09
PB - American Chemical Society (ACS)
SP - 57-63
IS - 1
VL - 109
PMID - 16839089
SN - 1089-5639
SN - 1520-5215
ER -
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@article{2004_Bernatowicz,
author = {Piotr Bernatowicz and Jozef Kowalewski and Dick Sandström},
title = {NMR Relaxation Study of the Protonated Form of 1,8-Bis(dimethylamino)naphthalene in Isotropic Solution: Anisotropic Motion outside of Extreme Narrowing and Ultrafast Proton Transfer},
journal = {Journal of Physical Chemistry A},
year = {2004},
volume = {109},
publisher = {American Chemical Society (ACS)},
month = {dec},
url = {https://doi.org/10.1021/jp045454n},
number = {1},
pages = {57--63},
doi = {10.1021/jp045454n}
}
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Bernatowicz, Piotr, et al. “NMR Relaxation Study of the Protonated Form of 1,8-Bis(dimethylamino)naphthalene in Isotropic Solution: Anisotropic Motion outside of Extreme Narrowing and Ultrafast Proton Transfer.” Journal of Physical Chemistry A, vol. 109, no. 1, Dec. 2004, pp. 57-63. https://doi.org/10.1021/jp045454n.