Journal of Physical Chemistry B, volume 108, issue 33, pages 12429-12435
Synthesis and Characterization of Colloidal CuInS2 Nanoparticles from a Molecular Single-Source Precursor
Stephanie L Castro
1
,
Sheila G. Bailey
1
,
Ryne P. Raffaelle
1
,
Kulbinder K Banger
1
,
Aloysius F. Hepp
1
1
Ohio Aerospace Institute, Cleveland, Ohio 44142, Photovoltaics and Space Environments Branch, NASA Glenn Research Center, Cleveland, Ohio 44135, and Department of Physics, Rochester Institute of Technology, Rochester, New York 14623
|
Publication type: Journal Article
Publication date: 2004-07-27
Journal:
Journal of Physical Chemistry B
Q1
Q3
SJR: 0.760
CiteScore: 5.8
Impact factor: 2.8
ISSN: 15206106, 15205207, 10895647
Materials Chemistry
Surfaces, Coatings and Films
Physical and Theoretical Chemistry
Abstract
Thermal decomposition of the molecular single-source precursor (PPh3)2CuIn(SEt)4 in the presence of hexanethiol in dioctylphthalate forms colloidal CuInS2 at 200 °C. The colloidal solution displays size-dependent quantum confinement behavior in the absorption and photoluminescence spectra. The average size of the nanocrystals can be increased from 2 to 4 nm by raising the reaction temperature from 200 °C to 250 °C. The nanoparticles are capped with hexanethiol ligands; these ligands can be exchanged with trioctylphosphine oxide or pyridine. The nature of the surface-capping ligands has a significant effect on the photoluminescence emission intensity. Investigation of the effect of synthesis parameters and postsynthesis treatments on the optical properties of the nanocrystals leads to the conclusion that the room-temperature emission originates in donor−acceptor defects.
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Castro S. L. et al. Synthesis and Characterization of Colloidal CuInS2 Nanoparticles from a Molecular Single-Source Precursor // Journal of Physical Chemistry B. 2004. Vol. 108. No. 33. pp. 12429-12435.
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Castro S. L., Bailey S. G., Raffaelle R. P., Banger K. K., Hepp A. F. Synthesis and Characterization of Colloidal CuInS2 Nanoparticles from a Molecular Single-Source Precursor // Journal of Physical Chemistry B. 2004. Vol. 108. No. 33. pp. 12429-12435.
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TY - JOUR
DO - 10.1021/jp049107p
UR - https://doi.org/10.1021/jp049107p
TI - Synthesis and Characterization of Colloidal CuInS2 Nanoparticles from a Molecular Single-Source Precursor
T2 - Journal of Physical Chemistry B
AU - Castro, Stephanie L
AU - Bailey, Sheila G.
AU - Raffaelle, Ryne P.
AU - Banger, Kulbinder K
AU - Hepp, Aloysius F.
PY - 2004
DA - 2004/07/27
PB - American Chemical Society (ACS)
SP - 12429-12435
IS - 33
VL - 108
SN - 1520-6106
SN - 1520-5207
SN - 1089-5647
ER -
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@article{2004_Castro,
author = {Stephanie L Castro and Sheila G. Bailey and Ryne P. Raffaelle and Kulbinder K Banger and Aloysius F. Hepp},
title = {Synthesis and Characterization of Colloidal CuInS2 Nanoparticles from a Molecular Single-Source Precursor},
journal = {Journal of Physical Chemistry B},
year = {2004},
volume = {108},
publisher = {American Chemical Society (ACS)},
month = {jul},
url = {https://doi.org/10.1021/jp049107p},
number = {33},
pages = {12429--12435},
doi = {10.1021/jp049107p}
}
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Castro, Stephanie L., et al. “Synthesis and Characterization of Colloidal CuInS2 Nanoparticles from a Molecular Single-Source Precursor.” Journal of Physical Chemistry B, vol. 108, no. 33, Jul. 2004, pp. 12429-12435. https://doi.org/10.1021/jp049107p.