Robust and Operationally Simple Synthesis of Poly(bis(2,2,2-trifluoroethoxy) phosphazene) with Controlled Molecular Weight, Low PDI, and High Conversion
Тип публикации: Journal Article
Дата публикации: 2014-05-29
SCImago Q1
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WOS Q2
БС1
SJR: 1.128
CiteScore: 8.8
Impact factor: 4.9
ISSN: 21611653
PubMed ID:
35590724
Materials Chemistry
Organic Chemistry
Inorganic Chemistry
Polymers and Plastics
Краткое описание
Synthetically straightforward conditions have been developed for the preparation of poly(bis 2,2,2-trifluoroethoxy)phosphazene with low PDI (<1.15) at high conversion (75-99%) and on a multigram scale. A combination of 31P NMR and GPC analyses demonstrate that molecular weight increases linearly as a function of monomer consumption, exhibiting first order kinetics with respect to monomer concentration up to high monomer conversion. Thus, the molecular weight can be controlled by varying the initiator (H2O) to monomer ratio.
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Steinke J. H. et al. Robust and Operationally Simple Synthesis of Poly(bis(2,2,2-trifluoroethoxy) phosphazene) with Controlled Molecular Weight, Low PDI, and High Conversion // ACS Macro Letters. 2014. Vol. 3. No. 6. pp. 548-551.
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Steinke J. H., Greenland B. W., Johns S., Parker M. P., Atkinson R. C. J., Cade I. A., Golding P., Trussell S. J. Robust and Operationally Simple Synthesis of Poly(bis(2,2,2-trifluoroethoxy) phosphazene) with Controlled Molecular Weight, Low PDI, and High Conversion // ACS Macro Letters. 2014. Vol. 3. No. 6. pp. 548-551.
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TY - JOUR
DO - 10.1021/mz500199x
UR - https://doi.org/10.1021/mz500199x
TI - Robust and Operationally Simple Synthesis of Poly(bis(2,2,2-trifluoroethoxy) phosphazene) with Controlled Molecular Weight, Low PDI, and High Conversion
T2 - ACS Macro Letters
AU - Steinke, Joachim H.G
AU - Greenland, Barnaby W
AU - Johns, Stephen
AU - Parker, Matthew P
AU - Atkinson, Robert C J
AU - Cade, Ian A.
AU - Golding, Peter
AU - Trussell, Stephen J
PY - 2014
DA - 2014/05/29
PB - American Chemical Society (ACS)
SP - 548-551
IS - 6
VL - 3
PMID - 35590724
SN - 2161-1653
ER -
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@article{2014_Steinke,
author = {Joachim H.G Steinke and Barnaby W Greenland and Stephen Johns and Matthew P Parker and Robert C J Atkinson and Ian A. Cade and Peter Golding and Stephen J Trussell},
title = {Robust and Operationally Simple Synthesis of Poly(bis(2,2,2-trifluoroethoxy) phosphazene) with Controlled Molecular Weight, Low PDI, and High Conversion},
journal = {ACS Macro Letters},
year = {2014},
volume = {3},
publisher = {American Chemical Society (ACS)},
month = {may},
url = {https://doi.org/10.1021/mz500199x},
number = {6},
pages = {548--551},
doi = {10.1021/mz500199x}
}
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MLA
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Steinke, Joachim H.G, et al. “Robust and Operationally Simple Synthesis of Poly(bis(2,2,2-trifluoroethoxy) phosphazene) with Controlled Molecular Weight, Low PDI, and High Conversion.” ACS Macro Letters, vol. 3, no. 6, May. 2014, pp. 548-551. https://doi.org/10.1021/mz500199x.
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