Tetrabutylammonium Salt Induced Denitration of Nitropyridines: Synthesis of Fluoro-, Hydroxy-, and Methoxypyridines
Тип публикации: Journal Article
Дата публикации: 2005-01-22
scimago Q1
wos Q1
БС1
SJR: 1.235
CiteScore: 8.7
Impact factor: 5
ISSN: 15237060, 15237052
PubMed ID:
15704898
Organic Chemistry
Biochemistry
Physical and Theoretical Chemistry
Краткое описание
An efficient method for the synthesis of fluoropyridines via the fluorodenitration reaction is reported. The reaction is mediated by tetrabutylammonium fluoride (TBAF) under mild conditions without undue regard to the presence of water. The fluorodenitration is general for 2- or 4-nitro-substituted pyridines, while 3-nitropyridines require attendant electron-withdrawing groups for the reaction to proceed efficiently. Nitropyridines also undergo hydroxy- and methoxydenitration under mild conditions in the presence of the corresponding tetrabutylammonium species.
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Kuduk S. D., DIPARDO R. M., BOCK M. G. Tetrabutylammonium Salt Induced Denitration of Nitropyridines: Synthesis of Fluoro-, Hydroxy-, and Methoxypyridines // Organic Letters. 2005. Vol. 7. No. 4. pp. 577-579.
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Kuduk S. D., DIPARDO R. M., BOCK M. G. Tetrabutylammonium Salt Induced Denitration of Nitropyridines: Synthesis of Fluoro-, Hydroxy-, and Methoxypyridines // Organic Letters. 2005. Vol. 7. No. 4. pp. 577-579.
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TY - JOUR
DO - 10.1021/ol047688v
UR - https://doi.org/10.1021/ol047688v
TI - Tetrabutylammonium Salt Induced Denitration of Nitropyridines: Synthesis of Fluoro-, Hydroxy-, and Methoxypyridines
T2 - Organic Letters
AU - Kuduk, Scott D.
AU - DIPARDO, ROBERT M.
AU - BOCK, MARK G.
PY - 2005
DA - 2005/01/22
PB - American Chemical Society (ACS)
SP - 577-579
IS - 4
VL - 7
PMID - 15704898
SN - 1523-7060
SN - 1523-7052
ER -
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@article{2005_Kuduk,
author = {Scott D. Kuduk and ROBERT M. DIPARDO and MARK G. BOCK},
title = {Tetrabutylammonium Salt Induced Denitration of Nitropyridines: Synthesis of Fluoro-, Hydroxy-, and Methoxypyridines},
journal = {Organic Letters},
year = {2005},
volume = {7},
publisher = {American Chemical Society (ACS)},
month = {jan},
url = {https://doi.org/10.1021/ol047688v},
number = {4},
pages = {577--579},
doi = {10.1021/ol047688v}
}
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MLA
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Kuduk, Scott D., et al. “Tetrabutylammonium Salt Induced Denitration of Nitropyridines: Synthesis of Fluoro-, Hydroxy-, and Methoxypyridines.” Organic Letters, vol. 7, no. 4, Jan. 2005, pp. 577-579. https://doi.org/10.1021/ol047688v.