Organic Letters

, том 14 , издание 10 , страницы 2468-2471

Organocatalytic Sequential α-Amination/Corey–Chaykovsky Reaction of Aldehydes: A High Yield Synthesis of 4-Hydroxypyrazolidine Derivatives

Тип публикации: Journal Article

Дата публикации: 2012-05-04

American Chemical Society (ACS)

Organic Letters

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SJR: 1.235

CiteScore: 8.7

Impact factor: 5

ISSN: 15237060, 15237052

DOI: 10.1021/ol300739b

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PubMed ID: 22559160

Organic Chemistry

Biochemistry

Physical and Theoretical Chemistry

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A tandem reaction of in situ generated α-amino aldehydes with dimethyloxosulfonium methylide under Corey-Chaykovsky reaction conditions proceeds efficiently to give 4-hydroxypyrazolidine derivatives in high yields with excellent enantio- and diastereoselectivities. This organocatalytic sequential method provides for the efficient synthesis of anti-1,2-aminoalcohols, structural subunits present in several bioactive molecules as well.

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Kumar B. S., Venkataramasubramanian V., Sudalai A. Organocatalytic Sequential α-Amination/Corey–Chaykovsky Reaction of Aldehydes: A High Yield Synthesis of 4-Hydroxypyrazolidine Derivatives // Organic Letters. 2012. Vol. 14. No. 10. pp. 2468-2471.

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TY - JOUR

DO - 10.1021/ol300739b

UR - https://doi.org/10.1021/ol300739b

TI - Organocatalytic Sequential α-Amination/Corey–Chaykovsky Reaction of Aldehydes: A High Yield Synthesis of 4-Hydroxypyrazolidine Derivatives

T2 - Organic Letters

AU - Kumar, B. Senthil

AU - Venkataramasubramanian, V

AU - Sudalai, Arumugam

PY - 2012

DA - 2012/05/04

PB - American Chemical Society (ACS)

SP - 2468-2471

IS - 10

VL - 14

PMID - 22559160

SN - 1523-7060

SN - 1523-7052

ER -

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@article{2012_Kumar,

author = {B. Senthil Kumar and V Venkataramasubramanian and Arumugam Sudalai},

title = {Organocatalytic Sequential α-Amination/Corey–Chaykovsky Reaction of Aldehydes: A High Yield Synthesis of 4-Hydroxypyrazolidine Derivatives},

journal = {Organic Letters},

year = {2012},

volume = {14},

publisher = {American Chemical Society (ACS)},

month = {may},

url = {https://doi.org/10.1021/ol300739b},

number = {10},

pages = {2468--2471},

doi = {10.1021/ol300739b}

}

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Kumar, B. Senthil, et al. “Organocatalytic Sequential α-Amination/Corey–Chaykovsky Reaction of Aldehydes: A High Yield Synthesis of 4-Hydroxypyrazolidine Derivatives.” Organic Letters, vol. 14, no. 10, May. 2012, pp. 2468-2471. https://doi.org/10.1021/ol300739b.