Zirconium complexes involving 2-phosphorus-substituted indenyl fragments
Denis N Kazulkin
1
,
Alexey N. Ryabov
1
,
Vyatcheslav V. Izmer
1
,
Carol M. Burns
1
,
Carol J Burns
1
,
Alexander Z. Voskoboynikov
1
1
Department of Chemistry, Moscow State University, Leninskie Gory, GSP-2, Moscow, 119992, Russian Federation, N. S. Kurnakov Institute of General and Inorganic Chemistry, 31 Leninsky Avenue, Moscow, 119991, Russian Federation, and Los Alamos National Laboratory, Chemical Division MS J515, Los Alamos, New Mexico 87545
|
Publication type: Journal Article
Publication date: 2005-05-11
scimago Q2
wos Q1
SJR: 0.676
CiteScore: 5.1
Impact factor: 2.9
ISSN: 02767333, 15206041
Organic Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
A series of 2-R2P-substituted indenes, where R2P = Ph2P, Cy2P, iPr2P, and tBu(H)P, were obtained via Pd-catalyzed reactions of 2-bromo-1H-indene (or 1H-inden-2-yl trifluoromethane sulfonate) with R2PH/Et3N. Analogous indenes bearing Me2P, tBu(Cl)P, and tBu2P substituents at position 2 were obtained through the reaction of 1H-inden-2-ylphosphonous dichloride with MeLi, tBuMgCl, and tBuMgCl/tBuLi−CuCN, respectively. Diethyl 1H-inden-2-ylphosphonate, prepared via the Ni-catalyzed Arbuzov reaction of 2-bromo-1H-indene with P(OEt)3, was found to be a convenient starting material for the synthesis of 2-H2P-substituted indene. 1H-Inden-2-yl(phenyl)phosphine, prepared via the Pd-catalyzed arylation of 2-H2P-substituted indene by PhI, turned out to react with 2-bromo-1H-indene in the presence of Pd(PPh3)4 and Et3N to form di(1H-inden-2-yl)(phenyl)phosphine in almost quantitative yield. Analogously, di(1H-inden-2-yl)(tert-butyl)phosphine was prepared via catalytic reaction of tBuPH2 with 2 equiv of 2-bromo-1H-inden...
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GOST
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Kazulkin D. N. et al. Zirconium complexes involving 2-phosphorus-substituted indenyl fragments // Organometallics. 2005. Vol. 24. No. 12. pp. 3024-3035.
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Kazulkin D. N., Ryabov A. N., Izmer V. V., Churakov A. V., Beletskaya I. P., Burns C., Burns C. J., Voskoboynikov A. Z. Zirconium complexes involving 2-phosphorus-substituted indenyl fragments // Organometallics. 2005. Vol. 24. No. 12. pp. 3024-3035.
Cite this
RIS
Copy
TY - JOUR
DO - 10.1021/om050236h
UR - https://pubs.acs.org/doi/10.1021/om050236h
TI - Zirconium complexes involving 2-phosphorus-substituted indenyl fragments
T2 - Organometallics
AU - Kazulkin, Denis N
AU - Ryabov, Alexey N.
AU - Izmer, Vyatcheslav V.
AU - Churakov, Andrei V.
AU - Beletskaya, Irina P.
AU - Burns, Carol M.
AU - Burns, Carol J
AU - Voskoboynikov, Alexander Z.
PY - 2005
DA - 2005/05/11
PB - American Chemical Society (ACS)
SP - 3024-3035
IS - 12
VL - 24
SN - 0276-7333
SN - 1520-6041
ER -
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BibTex (up to 50 authors)
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@article{2005_Kazulkin,
author = {Denis N Kazulkin and Alexey N. Ryabov and Vyatcheslav V. Izmer and Andrei V. Churakov and Irina P. Beletskaya and Carol M. Burns and Carol J Burns and Alexander Z. Voskoboynikov},
title = {Zirconium complexes involving 2-phosphorus-substituted indenyl fragments},
journal = {Organometallics},
year = {2005},
volume = {24},
publisher = {American Chemical Society (ACS)},
month = {may},
url = {https://pubs.acs.org/doi/10.1021/om050236h},
number = {12},
pages = {3024--3035},
doi = {10.1021/om050236h}
}
Cite this
MLA
Copy
Kazulkin, Denis N., et al. “Zirconium complexes involving 2-phosphorus-substituted indenyl fragments.” Organometallics, vol. 24, no. 12, May. 2005, pp. 3024-3035. https://pubs.acs.org/doi/10.1021/om050236h.
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