Di- and triphenylacetates of lanthanum and neodymium. Synthesis, structural diversity, and application in diene polymerization
Тип публикации: Journal Article
Дата публикации: 2013-02-19
scimago Q2
wos Q1
БС1
SJR: 0.676
CiteScore: 5.1
Impact factor: 2.9
ISSN: 02767333, 15206041
Organic Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Краткое описание
A new family of lanthanide complexes with di- and triphenylacetate ligands was prepared from LnCl3. Dimeric diphenylacetates were the only isolated products of the reaction between LnCl3 (Ln = La, Nd) and Ph2CHCOONa. The exchange reaction between LnCl3 and Ph3CCOONa led to the formation of three structurally different types of neodymium and lanthanum complexes under different reaction conditions. Various coordination modes of the carboxylate ligands were revealed, including κ2- and κ1-terminal coordination, μ2-κ1:κ1-bridging, and μ2-κ1:κ2-semibridging. The treatment of La and Nd tris-triphenylacetates with excess AlEt3 produces the dimeric tetraethylaluminates [Ln2((μ2-κ1:κ1-Ph3CCOO)4(AlEt4)2]. The structures of the key La and Nd triphenylacetates that were obtained from these reactions were verified by X-ray diffraction, and the complex [(THF)4Nd2(Ph2CHCOO)2(μ2-κ1:κ2-Ph2CHCOO)2(μ2- κ1:κ1-Ph2CHCOO)2] was studied by high-resolution X-ray diffraction. Neodymium di- and triphenylacetate complexes can serve a...
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Roitershtein D. M. et al. Di- and triphenylacetates of lanthanum and neodymium. Synthesis, structural diversity, and application in diene polymerization // Organometallics. 2013. Vol. 32. No. 5. pp. 1272-1286.
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Roitershtein D. M., Vinogradov A. A., Vinogradov A. A., Lyssenko K. A., Nelyubina Y. V., Ananev I. V., Nifant'ev I. E., Yakovlev V. A., Kostitsyna N. N. Di- and triphenylacetates of lanthanum and neodymium. Synthesis, structural diversity, and application in diene polymerization // Organometallics. 2013. Vol. 32. No. 5. pp. 1272-1286.
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TY - JOUR
DO - 10.1021/om301020r
UR - https://pubs.acs.org/doi/10.1021/om301020r
TI - Di- and triphenylacetates of lanthanum and neodymium. Synthesis, structural diversity, and application in diene polymerization
T2 - Organometallics
AU - Roitershtein, Dmitrii M.
AU - Vinogradov, Alexander A
AU - Vinogradov, Alexei A
AU - Lyssenko, Konstantin A.
AU - Nelyubina, Yulia V.
AU - Ananev, Ivan V
AU - Nifant'ev, Ilya E.
AU - Yakovlev, Vladimir A.
AU - Kostitsyna, Natalya N
PY - 2013
DA - 2013/02/19
PB - American Chemical Society (ACS)
SP - 1272-1286
IS - 5
VL - 32
SN - 0276-7333
SN - 1520-6041
ER -
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@article{2013_Roitershtein,
author = {Dmitrii M. Roitershtein and Alexander A Vinogradov and Alexei A Vinogradov and Konstantin A. Lyssenko and Yulia V. Nelyubina and Ivan V Ananev and Ilya E. Nifant'ev and Vladimir A. Yakovlev and Natalya N Kostitsyna},
title = {Di- and triphenylacetates of lanthanum and neodymium. Synthesis, structural diversity, and application in diene polymerization},
journal = {Organometallics},
year = {2013},
volume = {32},
publisher = {American Chemical Society (ACS)},
month = {feb},
url = {https://pubs.acs.org/doi/10.1021/om301020r},
number = {5},
pages = {1272--1286},
doi = {10.1021/om301020r}
}
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Roitershtein, Dmitrii M., et al. “Di- and triphenylacetates of lanthanum and neodymium. Synthesis, structural diversity, and application in diene polymerization.” Organometallics, vol. 32, no. 5, Feb. 2013, pp. 1272-1286. https://pubs.acs.org/doi/10.1021/om301020r.